(E)-N-(1-(4-methoxybenzyl)pyrrolidin-2-ylidene)-4-methylbenzenesulfonamide

Base Information

Chemical Name:(E)-N-(1-(4-methoxybenzyl)pyrrolidin-2-ylidene)-4-methylbenzenesulfonamide
CAS No.:131657-51-7
Molecular Formula:C₁₉H₂₂N₂O₃S
Molecular Weight:358.461
Hs Code.:

Synonyms:(E)-N-(1-(4-methoxybenzyl)pyrrolidin-2-ylidene)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(1-(4-methoxybenzyl)pyrrolidin-2-ylidene)-4-methylbenzenesulfonamide

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Technology Process of (E)-N-(1-(4-methoxybenzyl)pyrrolidin-2-ylidene)-4-methylbenzenesulfonamide

There total 2 articles about (E)-N-(1-(4-methoxybenzyl)pyrrolidin-2-ylidene)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 60737-65-7
1-(p-methoxybenzyl)-2-pyrrolidinone

: 4083-64-1
Tosyl isocyanate

: 131657-51-7
(E)-N-(1-(4-methoxybenzyl)pyrrolidin-2-ylidene)-4-methylbenzenesulfonamide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/jo00004a035

Reference yield: 65.0%

: 941-55-9
4-toluenesulfonyl azide

: 123-11-5
4-methoxy-benzaldehyde

: 609-36-9,25191-13-3,37159-97-0,4305-67-3,4607-28-7
rac-Pro-OH

: 131657-51-7
(E)-N-(1-(4-methoxybenzyl)pyrrolidin-2-ylidene)-4-methylbenzenesulfonamide

Guidance literature:: In ethanol; at 110 ℃; for 2h; Sealed tube;
DOI:10.1021/acs.orglett.0c04187

Reference yield:

: 131657-51-7
(E)-N-(1-(4-methoxybenzyl)pyrrolidin-2-ylidene)-4-methylbenzenesulfonamide

: 100-52-7
benzaldehyde

: 131657-69-7,131657-70-0
rel-(3S,1'S)-1-(4-methoxybenzyl)-3-(1-hydroxybenzyl)-2-(((4-methylphenyl)sulfonyl)imino)pyrrolidine

: 131657-69-7,131657-70-0
rel-(3S,1'R)-1-(4-methoxybenzyl)-3-(1-hydroxybenzyl)-2-(((4-methylphenyl)sulfonyl)imino)pyrrolidine

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h; Yield given. Yields of byproduct given;
DOI:10.1021/jo00004a035