C₂₅H₃₀Cl₂FN₃O₇

Base Information Edit

Chemical Name:C₂₅H₃₀Cl₂FN₃O₇
CAS No.:1040377-26-1
Molecular Formula:C₂₅H₃₀Cl₂FN₃O₇
Molecular Weight:574.434
Hs Code.:
Mol file:1040377-26-1.mol

C<sub>25</sub>H<sub>30</sub>Cl<sub>2</sub>FN<sub>3</sub>O<sub>7</sub>

Synonyms:C₂₅H₃₀Cl₂FN₃O₇

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Chemical Property of C₂₅H₃₀Cl₂FN₃O₇ Edit

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Technology Process of C₂₅H₃₀Cl₂FN₃O₇

There total 4 articles about C₂₅H₃₀Cl₂FN₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 64-17-5
ethanol

: 201230-82-2
carbon monoxide

: 1040377-24-9
C₂₂H₂₅Cl₃FN₃O₅

: 1040377-26-1
C₂₅H₃₀Cl₂FN₃O₇

Guidance literature:: With sodium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In N,N-dimethyl-formamide; at 90 ℃; for 1.5h;

Reference yield:

: 756520-66-8
1-(2,6-dichloro-3-fluorophenyl)ethanol

: 1040377-26-1
C₂₅H₃₀Cl₂FN₃O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

1.2: Reflux

2.1: dmap / N,N-dimethyl-formamide / 20 °C

3.1: sodium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 1.5 h / 90 °C

With dmap; sodium acetate; sodium hydride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 290835-85-7
2',6'-dichloro-3'-fluoroacetophenone

: 1040377-26-1
C₂₅H₃₀Cl₂FN₃O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

1.2: 0 °C / pH 6

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

2.2: Reflux

3.1: dmap / N,N-dimethyl-formamide / 20 °C

4.1: sodium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 1.5 h / 90 °C

With dmap; sodium tetrahydroborate; sodium acetate; sodium hydride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;