Cl₂InCH₂InCl₂((CH₂N(CH₃)2)2)2

Base Information

Chemical Name:Cl₂InCH₂InCl₂((CH₂N(CH₃)2)2)2
CAS No.:99666-60-1
Molecular Formula:C₁₃H₃₄Cl₄In₂N₄
Molecular Weight:617.892
Hs Code.:

Cl<sub>2</sub>InCH<sub>2</sub>InCl<sub>2</sub>((CH<sub>2</sub>N(CH<sub>3</sub>)2)2)2

Synonyms:Cl₂InCH₂InCl₂((CH₂N(CH₃)2)2)2

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Chemical Property of Cl₂InCH₂InCl₂((CH₂N(CH₃)2)2)2

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Technology Process of Cl₂InCH₂InCl₂((CH₂N(CH₃)2)2)2

There total 2 articles about Cl₂InCH₂InCl₂((CH₂N(CH₃)2)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 12672-70-7
indium chloride

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 10025-82-8
indium(III) chloride

: 7440-74-6
indium

: 99666-60-1
Cl₂InCH₂InCl₂((CH₂N(CH₃)2)2)2

: InCl₃*0.67(CH₂N(CH₃)2)2*0.67CH₂Cl₂

Guidance literature:: With methylene chloride; In dichloromethane; toluene; equimolar amts. of InCl and InCl3 suspended in CH2Cl2-toluene (1:1, v/v) at -80°C, TMEDA added, stirred, allowed to reach room temp., further stirred for 1 h (total react. time 3-4 h); filtered, crystals deposited on standing collected and dried under vac., further crop obtained by addn. of Et2O to mother liquor and recrystn. (CH2Cl2); InCl3 solvate isolated from separate expt. by addn. of petroleum ether to react. mixt.; elem. anal.;

Reference yield: 10.0%

: 12672-70-7
indium chloride

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 10025-82-8
indium(III) chloride

: 7440-74-6
indium

: 99666-60-1
Cl₂InCH₂InCl₂((CH₂N(CH₃)2)2)2

Guidance literature:: With methylene chloride; In dichloromethane; InCl and catalitic amts. of InCl3 suspended in CH2Cl2 at -80°C, TMEDA added, allowed to reach room temp. over ca. 2 h; Et2O added, ppt. collected, dried;