Technology Process of phenyl 4-(1H-1-tetrazolyl)phenylcarbamate
There total 7 articles about phenyl 4-(1H-1-tetrazolyl)phenylcarbamate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 0 ℃;
for 0.5h;
DOI:10.1248/cpb.48.1935
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 82 percent / K2CO3 / dimethylformamide / 32 h / 160 °C
2: 92 percent / N2H4*H2O; FeCl3; C* / methanol / 24 h / Heating
3: 68 percent / NaN3; AcOH / 4 h / 90 °C
4: H2; 6N aq. HCl / 10 percent Pd/C / methanol; tetrahydrofuran / 0.42 h / 20 °C
5: pyridine / ethyl acetate; tetrahydrofuran / 1 h / 20 °C
With
pyridine; hydrogenchloride; sodium azide; hydrogen; iron(III) chloride; potassium carbonate; pyrographite; hydrazine hydrate; acetic acid;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1248/cpb.48.1947
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 92 percent / N2H4*H2O; FeCl3; C* / methanol / 24 h / Heating
2: 68 percent / NaN3; AcOH / 4 h / 90 °C
3: H2; 6N aq. HCl / 10 percent Pd/C / methanol; tetrahydrofuran / 0.42 h / 20 °C
4: pyridine / ethyl acetate; tetrahydrofuran / 1 h / 20 °C
With
pyridine; hydrogenchloride; sodium azide; hydrogen; iron(III) chloride; pyrographite; hydrazine hydrate; acetic acid;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1248/cpb.48.1947
