1-deuteriodecane

Base Information

• Chemical Name: 1-deuteriodecane
• CAS No.: 71941-72-5
• Molecular Formula: C₁₀H₂₂
• Molecular Weight: 143.277
• Mol file: 71941-72-5.mol

Synonyms:1-deuteriodecane

Chemical Property of 1-deuteriodecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-deuteriodecane

There total 3 articles about 1-deuteriodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

1-Decene (872-05-9,17438-89-0,25189-70-2) → 3-methyleneundecane (71138-64-2) + 1-deuteriodecane (71941-72-5) + 3-(deuteriomethyl)undecane (133817-33-1)

Guidance literature:

With zirconocene dichloride; diclazuril; water-d2; triethylaluminum; In 1,2-dichloro-ethane;

DOI:10.1021/ja953655m

Reference yield: 37.0%

1-Decene (872-05-9,17438-89-0,25189-70-2) + triethylaluminum (97-93-8) → 3-methyleneundecane (71138-64-2) + 1-deuteriodecane (71941-72-5) + 3-(deuteriomethyl)undecane (133817-33-1)

Guidance literature:

With zirconocene dichloride; diclazuril; water-d2; In 1,2-dichloro-ethane;

DOI:10.1021/ja953655m

Reference yield: 11.0%

cis-5-decene (7433-78-5) → decane (124-18-5) + (E)-5-decene (7433-56-9) + trans-3-decene (19150-21-1) + (Z)-dec-4-ene (19398-88-0) + trans-4-Decen (19398-89-1) + 1-deuteriodecane (71941-72-5)

Guidance literature:

With Schwartz's reagent; water-d2; In toluene; at 40 ℃; for 4h; Product distribution; Mechanism; variation of time, amount of reagent, further olefins, deuterium labelling experiments;

DOI:10.1016/0022-328X(89)80053-1

upstream raw materials:

cis-5-decene

1-Decene

triethylaluminum