(1S,2S,3R,4R)-1,2,3-tris(benzyloxy)-4-[(benzyloxy)methyl]-6-methylidenecyclohexane

Base Information

Chemical Name:(1S,2S,3R,4R)-1,2,3-tris(benzyloxy)-4-[(benzyloxy)methyl]-6-methylidenecyclohexane
CAS No.:639852-45-2
Molecular Formula:C₃₆H₃₈O₄
Molecular Weight:534.695
Hs Code.:

Synonyms:(1S,2S,3R,4R)-1,2,3-tris(benzyloxy)-4-[(benzyloxy)methyl]-6-methylidenecyclohexane

Suppliers and Price of (1S,2S,3R,4R)-1,2,3-tris(benzyloxy)-4-[(benzyloxy)methyl]-6-methylidenecyclohexane

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Chemical Property of (1S,2S,3R,4R)-1,2,3-tris(benzyloxy)-4-[(benzyloxy)methyl]-6-methylidenecyclohexane

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Technology Process of (1S,2S,3R,4R)-1,2,3-tris(benzyloxy)-4-[(benzyloxy)methyl]-6-methylidenecyclohexane

There total 1 articles about (1S,2S,3R,4R)-1,2,3-tris(benzyloxy)-4-[(benzyloxy)methyl]-6-methylidenecyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 124330-57-0
(2R,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexanone

: 639852-45-2
(1S,2S,3R,4R)-1,2,3-tris(benzyloxy)-4-[(benzyloxy)methyl]-6-methylidenecyclohexane

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In hexane; at 0 ℃;

(2R,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexanone; In tetrahydrofuran; hexane; for 3h;
DOI:10.1002/hlca.200390178

Reference yield: 25.0%

: 639852-45-2
(1S,2S,3R,4R)-1,2,3-tris(benzyloxy)-4-[(benzyloxy)methyl]-6-methylidenecyclohexane

: 639852-51-0
(3S,4R,5S,6R,7R)-4,5,6-tris(benzyloxy)-7-[(benzyloxy)methyl]-1-oxaspiro[2.5]octane

: 639852-53-2
(3R,4R,5S,6R,7R)-4,5,6-tris(benzyloxy)-7-[(benzyloxy)methyl]-1-oxaspiro[2.5]octane

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 3.66667h;
DOI:10.1002/hlca.200390178