Diazene,1-butyl-2-phenyl-

Base Information

• Chemical Name: Diazene,1-butyl-2-phenyl-
• CAS No.: 940-55-6
• Molecular Formula: C10H14 N2
• Molecular Weight: 162.235
• Mol file: 940-55-6.mol

Synonyms:Benzeneazobutane(7CI,8CI); Diazene, butylphenyl- (9CI); Butaneazobenzene

Chemical Property of Diazene,1-butyl-2-phenyl-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Diazene,1-butyl-2-phenyl-

There total 3 articles about Diazene,1-butyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-butylamine (109-73-9,85404-21-3) + Nitrosobenzene (586-96-9) → aniline (62-53-3) + azoxybenzene (495-48-7,55599-32-1) + (phenylazo)-n-butane (940-55-6)

Guidance literature:

In methanol; for 35h; Ambient temperature;

DOI:10.1021/jo00203a024

Reference yield:

1-bromo-butane (109-65-9) + phenylhydrazine (100-63-0) → (phenylazo)-n-butane (940-55-6)

Guidance literature:

With diethyl ether; Behandeln des Reaktionsprodukts mit Quecksilber(II)-oxid in Aether;

DOI:10.1246/bcsj.10.169

Reference yield:

→ (phenylazo)-n-butane (940-55-6)

Guidance literature:

aus 1-Butyl-2-phenylhydrazin mit gelbem HgO/Et2O;

DOI:10.1039/jr9650002788

upstream raw materials:

1-bromo-butane

phenylhydrazine

N-butylamine

Nitrosobenzene