3,4-Dimethoxy-4'-nitrobenzophenone

Base Information

• Chemical Name: 3,4-Dimethoxy-4'-nitrobenzophenone
• CAS No.: 97726-03-9
• Molecular Formula: C₁₅H₁₃NO₅
• Molecular Weight: 287.272

Synonyms:3,4-Dimethoxy-4'-nitrobenzophenone

Chemical Property of 3,4-Dimethoxy-4'-nitrobenzophenone

Chemical Property:

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Technology Process of 3,4-Dimethoxy-4'-nitrobenzophenone

There total 8 articles about 3,4-Dimethoxy-4'-nitrobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

3,4-dimethoxyphenylacetonitrile (93-17-4) + 4-chlorobenzonitrile (100-00-5) → 3,4-Dimethoxy-4'-nitrobenzophenone (97726-03-9) + 5-chloro-3-(3,4-dimethoxyphenyl)-2,1-benzisoxazole (94100-08-0) + 2-chloro-5,6-dimethoxyacridine-9-carbonitrile N-oxide (115764-95-9) + 2-(2-chloro-5-(hydroxyimino)-1,3-cyclohexadien-6-ylidene)-1,2-bis(3,4-dimethoxyphenyl)ethan-1-one (115764-96-0)

Guidance literature:

With potassium hydroxide; In methanol; water; benzene; for 3h; Ambient temperature;

Reference yield: 74.0%

(3-hydroxy-4-methoxyphenyl)(4-nitrophenyl)methanone (1449505-56-9) + dimethyl sulfate (77-78-1) → 3,4-Dimethoxy-4'-nitrobenzophenone (97726-03-9)

Guidance literature:

With potassium carbonate; In acetone; for 18h; Reflux;

DOI:10.1039/c2ra22391k

Reference yield: 71.0%

1,2-dimethoxybenzene (91-16-7) + 4-nitro-benzoyl chloride (122-04-3) → 3,4-Dimethoxy-4'-nitrobenzophenone (97726-03-9)

Guidance literature:

With aluminum (III) chloride; In 1,2-dichloro-ethane; at 20 ℃; Cooling with ice;

DOI:10.1002/ardp.201000312

upstream raw materials:

1,2-dimethoxybenzene

4-nitro-benzoyl chloride

3,4-dimethoxyphenylacetonitrile

4-chlorobenzonitrile

Downstream raw materials:

3-(3,4-Dimethoxyphenyl)-3-(4'-nitrophenyl)acrylonitrile

(4-aminophenyl)(3,4-dimethoxyphenyl)methanone

(4-amino-3-iodophenyl)(3,4-dimethoxyphenyl)methanone

2-amino-5-(3,4-dimethoxybenzoyl)-benzonitrile

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