Technology Process of 3-acetamido-4-ethoxybenzoic acid
There total 4 articles about 3-acetamido-4-ethoxybenzoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 60 - 62 ℃;
for 2h;
Reagent/catalyst;
Solvent;
- Guidance literature:
-
methyl 3-acetamido-4-ethoxybenzoate;
With
sodium hydroxide;
In
methanol; water;
at 20 ℃;
for 5h;
Large scale reaction;
With
hydrogenchloride;
In
water;
at 20 ℃;
pH=2 - 3;
DOI:10.3987/COM-11-12343
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: acetic acid / 3 h / 60 °C / Large scale reaction
2.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 60 °C / Large scale reaction
3.1: sodium hydroxide / methanol; water / 5 h / 20 °C / Large scale reaction
3.2: 20 °C / pH 2 - 3
With
potassium carbonate; acetic acid; sodium hydroxide;
In
methanol; water; N,N-dimethyl-formamide;
DOI:10.3987/COM-11-12343
