N-benzyloxycarbonyl-N'-(4-[dimethylazaniumylidene]-1,4-dihydropyridin-1-ylsulfonyl)azanide

Base Information

• Chemical Name: N-benzyloxycarbonyl-N'-(4-[dimethylazaniumylidene]-1,4-dihydropyridin-1-ylsulfonyl)azanide
• CAS No.: 1037211-09-8
• Molecular Formula: C₁₅H₁₇N₃O₄S
• Molecular Weight: 335.384
• Mol file: 1037211-09-8.mol

Synonyms:N-benzyloxycarbonyl-N'-(4-[dimethylazaniumylidene]-1,4-dihydropyridin-1-ylsulfonyl)azanide

Chemical Property of N-benzyloxycarbonyl-N'-(4-[dimethylazaniumylidene]-1,4-dihydropyridin-1-ylsulfonyl)azanide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzyloxycarbonyl-N'-(4-[dimethylazaniumylidene]-1,4-dihydropyridin-1-ylsulfonyl)azanide

There total 1 articles about N-benzyloxycarbonyl-N'-(4-[dimethylazaniumylidene]-1,4-dihydropyridin-1-ylsulfonyl)azanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

dmap (1122-58-3) + isocyanate de chlorosulfonyle (1189-71-5) + benzyl alcohol (100-51-6,185532-71-2) → N-benzyloxycarbonyl-N'-(4-[dimethylazaniumylidene]-1,4-dihydropyridin-1-ylsulfonyl)azanide (1037211-09-8)

Guidance literature:

isocyanate de chlorosulfonyle; benzyl alcohol; In dichloromethane; at 0 ℃; for 0.166667h;

dmap; In dichloromethane; at 20 ℃;

Reference yield: 90.0%

N-benzyloxycarbonyl-N'-(4-[dimethylazaniumylidene]-1,4-dihydropyridin-1-ylsulfonyl)azanide (1037211-09-8) + 2,2-diphenyl-4-pentenylamine (53001-06-2) → benzyl N-(2,2-diphenylpent-4-en-1-yl)sulfamoylcarbamate (958264-13-6)

Guidance literature:

In dichloromethane; Inert atmosphere; Schlenk technique;

DOI:10.1002/chem.201403891

Reference yield: 90.0%

N-benzyloxycarbonyl-N'-(4-[dimethylazaniumylidene]-1,4-dihydropyridin-1-ylsulfonyl)azanide (1037211-09-8) + 2,2-dimethyl-1-amino-pent-4-ene (73604-46-3) → benzyl N-(2,2-dimethylpent-4-en-1-yl)sulfamoylcarbamate (958264-16-9)

Guidance literature:

In dichloromethane; Inert atmosphere; Schlenk technique;

DOI:10.1002/chem.201403891

upstream raw materials:

dmap

isocyanate de chlorosulfonyle

benzyl alcohol

Downstream raw materials:

benzyl N-(2,2,4-triphenylpent-4-en-1-yl)sulfamoylcarbamate

C₂₄H₃₀N₂O₄S

benzyl N-(2,2-dimethylpent-4-en-1-yl)sulfamoylcarbamate

benzyl N-(2,2-diphenylpent-4-en-1-yl)sulfamoylcarbamate