(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)trichloridoaluminum

Base Information

Chemical Name:(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)trichloridoaluminum
CAS No.:1197159-88-8
Molecular Formula:C₂₁H₂₆AlCl₃N₂
Molecular Weight:439.791
Hs Code.:

Synonyms:(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)trichloridoaluminum

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Chemical Property of (1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)trichloridoaluminum

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Technology Process of (1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)trichloridoaluminum

There total 5 articles about (1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)trichloridoaluminum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 7446-70-0
aluminium trichloride

: 173035-11-5
1,3-bis(2,4,6-trimethylphenyl)imidazolidin-2-ylidene

: 1197159-88-8
(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)trichloridoaluminum

Guidance literature:: In benzene; (N2), suspn. of ligand in benzene treated with 1 equiv. of AlCl3 stirredfor 3 h; evapd., dried (vac.), recrystd.(CH2Cl2/Et2O), elem. anal.;
DOI:10.1002/ejic.200801161

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: C₂₁H₂₆AlF₃N₂

: 420-56-4
trimethylsilyl fluoride

: 1197159-88-8
(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)trichloridoaluminum

Guidance literature:: In benzene-d6; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejic.201900921

Reference yield:

: 173035-11-5
1,3-bis(2,4,6-trimethylphenyl)imidazolidin-2-ylidene

: 1197159-88-8
(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)trichloridoaluminum

Guidance literature:: Multi-step reaction with 3 steps

1.1: ⁽²⁾H₈-toluene / 0.08 h / Inert atmosphere

1.2: Inert atmosphere

2.1: toluene / 2 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: benzene-d6 / 1 h / 20 °C / Inert atmosphere

In benzene-d6; ⁽²⁾H₈-toluene; toluene;
DOI:10.1002/ejic.201900921