benzyl trans-3-hydroxy-3-methylcyclobutanecarboxylate

Base Information

Chemical Name:benzyl trans-3-hydroxy-3-methylcyclobutanecarboxylate
CAS No.:1303609-20-2
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:

Synonyms:benzyl trans-3-hydroxy-3-methylcyclobutanecarboxylate

Suppliers and Price of benzyl trans-3-hydroxy-3-methylcyclobutanecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of benzyl trans-3-hydroxy-3-methylcyclobutanecarboxylate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of benzyl trans-3-hydroxy-3-methylcyclobutanecarboxylate

There total 8 articles about benzyl trans-3-hydroxy-3-methylcyclobutanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 676-58-4
methylmagnesium chloride

: 198995-91-4
benzyl 3-oxocyclobutane-1-carboxylate

: 1303609-20-2
benzyl trans-3-hydroxy-3-methylcyclobutanecarboxylate

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201500746

Reference yield:

: 676-58-4
methylmagnesium chloride

: 198995-91-4
benzyl 3-oxocyclobutane-1-carboxylate

: benzyl 3-hydroxy-3-methylcyclobutanecarboxylate

: 1303609-20-2
benzyl trans-3-hydroxy-3-methylcyclobutanecarboxylate

Guidance literature:: methylmagnesium chloride; benzyl 3-oxocyclobutane-1-carboxylate; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether;