3-acetoxy-2,5-dihydroxy-5-carboxy-2,3,5-trimethylpentan-4-olide

Base Information

• Chemical Name: 3-acetoxy-2,5-dihydroxy-5-carboxy-2,3,5-trimethylpentan-4-olide
• CAS No.: 109576-73-0
• Molecular Formula: C₁₁H₁₆O₈
• Molecular Weight: 276.243
• Mol file: 109576-73-0.mol

Synonyms:3-acetoxy-2,5-dihydroxy-5-carboxy-2,3,5-trimethylpentan-4-olide

Chemical Property of 3-acetoxy-2,5-dihydroxy-5-carboxy-2,3,5-trimethylpentan-4-olide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of 3-acetoxy-2,5-dihydroxy-5-carboxy-2,3,5-trimethylpentan-4-olide

There total 3 articles about 3-acetoxy-2,5-dihydroxy-5-carboxy-2,3,5-trimethylpentan-4-olide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.8%

2,4,5-trimethylphenol (496-78-6) + acetic acid (64-19-7,77671-22-8) → 2,3,5-trimethyl-1,6-benzoquinone (13038-87-4) + 2,4,5-trimethyl-1-acetoxybenzene (69305-42-6) + 1-methoxy-2,4,5-trimethylbenzene (21573-38-6) + 4-acetoxy-2,3,5-trimethylphenol (36592-62-8) + 3-acetoxy-2,5-dihydroxy-5-carboxy-2,3,5-trimethylpentan-4-olide (109576-73-0)

Guidance literature:

With peracetic acid; at 50 ℃; for 0.25h; Product distribution; Kinetics; Thermodynamic data;

Reference yield: 82.6%

1,2,4-Trimethylbenzene (95-63-6) + acetic acid (64-19-7,77671-22-8) → 2,3,5-Trimethyl-1,4-benzoquinone (935-92-2) + Duroquinone (527-17-3,70128-24-4) + 2,3,5-trimethylanisole (20469-61-8) + 2,3,6-trimethylphenyl acetate (62687-45-0) + 1-methoxy-2,4,5-trimethylbenzene (21573-38-6) + 3-acetoxy-2,5-dihydroxy-5-carboxy-2,3,5-trimethylpentan-4-olide (109576-73-0)

Guidance literature:

With peracetic acid; at 70 ℃; for 0.5h; Product distribution; Kinetics; Thermodynamic data; other reaction time: 4 h.;

Reference yield: 68.2%

2,3,5-trimethylphenol (697-82-5) + acetic acid (64-19-7,77671-22-8) → 2,3,5-Trimethyl-1,4-benzoquinone (935-92-2) + 2,3,5-trimethyl-1,6-benzoquinone (13038-87-4) + 2,3,5-trimethylanisole (20469-61-8) + 2,3,5-trimethyl-1-acetoxybenzene (34649-27-9) + 1-acetoxy-4-methoxy-2,3,5-trimethylbenzene + 3-acetoxy-2,5-dihydroxy-5-carboxy-2,3,5-trimethylpentan-4-olide (109576-73-0)

Guidance literature:

With peracetic acid; at 50 ℃; for 0.25h; Product distribution; Kinetics; Thermodynamic data;

upstream raw materials:

1,2,4-Trimethylbenzene

acetic acid

2,4,5-trimethylphenol

2,3,5-trimethylphenol