1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid

Base Information

Chemical Name:1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid
CAS No.:1395047-02-5
Molecular Formula:C₁₄H₁₃N₃O₄
Molecular Weight:287.275
Hs Code.:

Synonyms:1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid

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Chemical Property of 1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid

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Technology Process of 1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid

There total 4 articles about 1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1395047-01-4
1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester

: 1395047-02-5
1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid

Guidance literature:: 1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester; With lithium iodide; In ethyl acetate; for 4h; Reflux;

With hydrogenchloride; water; In ethyl acetate; pH=4;

Reference yield:

: 100-47-0
benzonitrile

: 1395047-02-5
1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / methanol / 12 h / 20 °C / Inert atmosphere

1.2: 0.33 h

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 6 h / 120 °C

3.1: toluene-4-sulfonic acid / ethanol / 4 h / Reflux

4.1: lithium iodide / ethyl acetate / 4 h / Reflux

4.2: pH 4

With sodium methylate; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium iodide; toluene-4-sulfonic acid; In methanol; ethanol; ethyl acetate; acetonitrile;

Reference yield:

: 308276-57-5
N-(2,2-dimethoxyethyl)benzamidine

: 1395047-02-5
1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 6 h / 120 °C

2.1: toluene-4-sulfonic acid / ethanol / 4 h / Reflux

3.1: lithium iodide / ethyl acetate / 4 h / Reflux

3.2: pH 4

With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium iodide; toluene-4-sulfonic acid; In ethanol; ethyl acetate; acetonitrile;