1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester

Base Information

Chemical Name:1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester
CAS No.:1395047-01-4
Molecular Formula:C₁₅H₁₅N₃O₄
Molecular Weight:301.302
Hs Code.:

Synonyms:1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester

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Chemical Property of 1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester

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Technology Process of 1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester

There total 3 articles about 1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 593-56-6
N-methoxylamine hydrochloride

: 308276-58-6
methyl 1-(2,2-dimethoxyethyl)-1,6-dihydro-6-oxo-2-phenyl-5-pyrimidinecarboxylate

: 1395047-01-4
1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester

Guidance literature:: N-methoxylamine hydrochloride; methyl 1-(2,2-dimethoxyethyl)-1,6-dihydro-6-oxo-2-phenyl-5-pyrimidinecarboxylate; toluene-4-sulfonic acid; In ethanol; for 4h; Reflux;

With sodium hydrogencarbonate; In ethanol; dichloromethane;

Reference yield:

: 100-47-0
benzonitrile

: 1395047-01-4
1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / methanol / 12 h / 20 °C / Inert atmosphere

1.2: 0.33 h

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 6 h / 120 °C

3.1: toluene-4-sulfonic acid / ethanol / 4 h / Reflux

With sodium methylate; 1,8-diazabicyclo[5.4.0]undec-7-ene; toluene-4-sulfonic acid; In methanol; ethanol; acetonitrile;

Reference yield:

: 308276-57-5
N-(2,2-dimethoxyethyl)benzamidine

: 1395047-01-4
1,6-dihydro-1-[2-(methoxyimino)ethyl]-6-oxo-2-phenyl-5-pyrimidinecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 6 h / 120 °C

2: toluene-4-sulfonic acid / ethanol / 4 h / Reflux

With 1,8-diazabicyclo[5.4.0]undec-7-ene; toluene-4-sulfonic acid; In ethanol; acetonitrile;