((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane

Base Information

Chemical Name:((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane
CAS No.:877203-77-5
Molecular Formula:C₂₂H₂₆Cl₂O₂Si
Molecular Weight:421.439
Hs Code.:

Synonyms:((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane

Chemical Property:

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Technology Process of ((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane

There total 1 articles about ((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 56-23-5
tetrachloromethane

: 87770-83-0
(Z)-4-((tert-butyldiphenylsilyl)oxy)but-2-en-1-ol

: 2258-42-6
formyl acetic anhydride

: 877203-77-5
((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane

Guidance literature:: (Z)-4-((tert-butyldiphenylsilyl)oxy)but-2-en-1-ol; formyl acetic anhydride; With pyridine; at 0 ℃;

tetrachloromethane; With triphenylphosphine; In tetrahydrofuran; at 60 ℃;
DOI:10.1021/ol052685j

Reference yield: 73.0%

: 877203-77-5
((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane

: 75-77-4
chloro-trimethyl-silane

: 64-17-5
ethanol

: 3-(tert-butyl-diphenyl-silanyloxymethyl)-2-trimethylsilanyl-pent-4-enoic acid ethyl ester

Guidance literature:: ((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -42 ℃;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - -40 ℃;

ethanol; In tetrahydrofuran; hexane; at -40 - 20 ℃;
DOI:10.1021/ol052685j

Reference yield: 56.0%

: 877203-77-5
((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane

: 64-17-5
ethanol

: 333-27-7
methyl trifluoromethanesulfonate

: 3-(tert-butyl-diphenyl-silanyloxymethyl)-2-methyl-pent-4-enoic acid ethyl ester

Guidance literature:: ((Z)-41-(2,2-dichlorovinyloxy)but-2-enyloxy)(tert-butyl)diphenylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -42 ℃;

methyl trifluoromethanesulfonate; In tetrahydrofuran; hexane; at -78 - -40 ℃;

ethanol; In tetrahydrofuran; hexane; at -40 - 20 ℃;
DOI:10.1021/ol052685j