N,N-Diethyl-N'-(4-methoxybenzylidene)ethylenediamine

Base Information

• Chemical Name: N,N-Diethyl-N'-(4-methoxybenzylidene)ethylenediamine
• CAS No.: 92492-99-4
• Molecular Formula: C₁₄H₂₂N₂O
• Molecular Weight: 234.341
• European Community (EC) Number: 666-382-1
• Mol file: 92492-99-4.mol

Synonyms:N,N-DIETHYL-N'-(4-METHOXYBENZYLIDENE)ETHYLENEDIAMINE;AKOS024336789

Chemical Property of N,N-Diethyl-N'-(4-methoxybenzylidene)ethylenediamine

Chemical Property:

• XLogP3: 2.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 7
• Exact Mass: 234.173213330
• Heavy Atom Count: 17
• Complexity: 206

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCN(CC)CCN=CC1=CC=C(C=C1)OC

Technology Process of N,N-Diethyl-N'-(4-methoxybenzylidene)ethylenediamine

There total 1 articles about N,N-Diethyl-N'-(4-methoxybenzylidene)ethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-methoxy-benzaldehyde (123-11-5) + N,N-diethylethylenediamine (100-36-7) → 2-(diethylamino)ethyl(4-methoxyphenyl)methylideneamine (92492-99-4)

Guidance literature:

With sodium sulfate; In methanol; for 24h; Reflux;

DOI:10.1002/chem.201501003

Reference yield: 96.0%

2-(diethylamino)ethyl(4-methoxyphenyl)methylideneamine (92492-99-4) + methyl iodide (74-88-4) → N,N-diethyl-N-methyl-4-(p-methoxyphenyl)-3-aza-3-butenylammonium iodide (126714-77-0)

Guidance literature:

Reference yield:

2-(diethylamino)ethyl(4-methoxyphenyl)methylideneamine (92492-99-4) → 2-Hydroxy-4-methoxybenzaldehyde (673-22-3) + 4-methoxy-benzaldehyde (123-11-5)

Guidance literature:

2-(diethylamino)ethyl(4-methoxyphenyl)methylideneamine; With tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate; oxygen; In acetone; at 20 ℃; for 0.5h; Glovebox;

With hydrogenchloride; In water; acetone; at 70 ℃; for 0.5h; Glovebox;

DOI:10.1002/chem.201501003

upstream raw materials:

4-methoxy-benzaldehyde

N,N-diethylethylenediamine

Downstream raw materials:

[2-(diethylamino)ethyl][(4-methoxyphenyl)methyl]amine

N,N-diethyl-N-methyl-4-(p-methoxyphenyl)-3-aza-3-butenylammonium iodide

1-(p-methoxyphenyl)-2-aza-1,3-butadiene

1-(p-methoxyphenyl)-3-methoxy-2-aza-1-butene