4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside
CAS No.:1095998-28-9
Molecular Formula:C₄₂H₃₂N₂O₉S₂
Molecular Weight:772.856
Hs Code.:

Synonyms:4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

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Technology Process of 4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

There total 1 articles about 4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 1095998-03-0
4-(pyridin-2'-yl)thiazole-2(3H)-thione sodium salt

: 1095998-28-9
4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

Guidance literature:: In acetonitrile; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1039/b810569c

Reference yield: 82.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1095998-28-9
4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

: 128503-39-9,143995-74-8,125084-78-8
methyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; for 17h; Molecular sieve; Inert atmosphere;
DOI:10.1039/b810569c

Reference yield: 54.0%

: 14104-20-2
silver tetrafluoroborate

: 1095998-28-9
4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

: fac-[(PtMe₃I)4]

: 67-64-1
acetone

: fac-[PtMe3(4-(pyridine-2-yl)-thiazole-2-yl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside)][BF4]

Guidance literature:: In acetone; byproducts: AgI; under Ar; a suspn. of Pt-contg. compd. (0.04 mmol) and AgBF4 (0.14 mmol)in acetone was stirred for 30 min under the absence of light; AgI was r emoved by filtration; a soln. of Pt-contg. compd. was added to the ligand (0.14 mmol); after 5 h the vol. of the soln. was reduced in vac. and pentane was added; the solid was filtered, washed with pentane and dried in vac.;
DOI:10.1039/b927058b