germane, methoxy-

Base Information

• Chemical Name: germane, methoxy-
• CAS No.: 5910-93-0
• Molecular Formula: CH₆GeO
• Molecular Weight: 106.648
• Mol file: 5910-93-0.mol

Synonyms:methoxygermane

Chemical Property of germane, methoxy-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of germane, methoxy-

There total 2 articles about germane, methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + ((CH3)3N)GeH3Br*(CH3)2O → germane (7782-65-2) + digermane (13818-89-8) + trigermane (14691-44-2) + digermyl ether (14939-17-4) + methoxygermane (5910-93-0)

Guidance literature:

In Dimethyl ether; byproducts: (CH3)3NHBr; MeOH was added to Me3N*GeH3Br*Me2O in Me2O, mixt. was warmed to -63°C for 4-5 h; volatiles were removed in vac., sepd. by low temp. high-vac. distn.;

DOI:10.1016/S0020-1693(00)90325-6

Reference yield:

(CH3)3NGeH3Br (60342-06-5) → trimethyl ammonium bromide (2840-24-6) + methoxygermane (5910-93-0)

Guidance literature:

With methanol; In neat (no solvent); under N2 or in vac., allowed to react at -63°C, reaction time: 6 h;

DOI:10.1016/S0020-1693(00)85155-5

upstream raw materials:

methanol

(CH₃)3NGeH₃Br