bis(biphenyl-4-yl)methanol

Base Information

Chemical Name:bis(biphenyl-4-yl)methanol
CAS No.:4596-95-6
Molecular Formula:C₂₅H₂₀O
Molecular Weight:336.433
Hs Code.:

Synonyms:bis(biphenyl-4-yl)methanol

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Chemical Property of bis(biphenyl-4-yl)methanol

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Technology Process of bis(biphenyl-4-yl)methanol

There total 28 articles about bis(biphenyl-4-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.6%

: 107-31-3
Methyl formate

: 92-66-0
4-bromo-1,1'-biphenyl

: 4596-95-6
bis(biphenyl-4-yl)methanol

Guidance literature:: 4-bromo-1,1'-biphenyl; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

Methyl formate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4.16667h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2018.01.055

Reference yield: 85.0%

: 92-66-0
4-bromo-1,1'-biphenyl

: 109-94-4
formic acid ethyl ester

: 4596-95-6
bis(biphenyl-4-yl)methanol

Guidance literature:: 4-bromo-1,1'-biphenyl; With iodine; magnesium; In tetrahydrofuran; for 2h; Reflux; Inert atmosphere;

formic acid ethyl ester; In tetrahydrofuran; at 20 ℃; for 2.08333h; Inert atmosphere;
DOI:10.1002/hc.20753

Reference yield: 49.0%

: 92-66-0
4-bromo-1,1'-biphenyl

: 109-94-4
formic acid ethyl ester

: 6301-56-0
ethyl 4-phenylbenzoate

: 4596-95-6
bis(biphenyl-4-yl)methanol

: 3218-36-8
4-Phenylbenzaldehyde

Guidance literature:: 4-bromo-1,1'-biphenyl; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

formic acid ethyl ester; In tetrahydrofuran; hexane; at -78 ℃; for 3h;

With ethanol; iodine; potassium carbonate; In hexane; at -78 - 20 ℃; for 18h;
DOI:10.1016/j.tet.2012.04.016