2,4,6-trifluorophenylmagnesium bromide

Base Information

Chemical Name:2,4,6-trifluorophenylmagnesium bromide
CAS No.:114318-52-4
Molecular Formula:C₆H₂BrF₃Mg
Molecular Weight:235.286
Hs Code.:

Synonyms:2,4,6-trifluorophenylmagnesium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4,6-trifluorophenylmagnesium bromide

Chemical Property:

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Technology Process of 2,4,6-trifluorophenylmagnesium bromide

There total 2 articles about 2,4,6-trifluorophenylmagnesium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2367-76-2
2,4,6-trifluorobromobenzene

: 927-77-5
n-propylmagnesium bromide

: 114318-52-4
2,4,6-trifluorophenylmagnesium bromide

Guidance literature:: In diethyl ether;

Reference yield:

: 2367-76-2
2,4,6-trifluorobromobenzene

: 114318-52-4
2,4,6-trifluorophenylmagnesium bromide

Guidance literature:

Reference yield: 74.7%

: 114318-52-4
2,4,6-trifluorophenylmagnesium bromide

: 7787-58-8
bismuth(III) bromide

: 186805-17-4
tris(2,4,6-trifluorophenyl)bismuth

Guidance literature:: In tetrahydrofuran; byproducts: MgBr2; N2 atm.; molar ratio BiBr3:RMgBr 1:3, cooling (-40°C), heating (to room temp.), stirring (2 h); evapn., extraction (n-hexane); elem. anal.;
DOI:10.1002/zaac.19966221202