1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester

Base Information

Chemical Name:1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester
CAS No.:1033586-29-6
Molecular Formula:C₁₃H₁₂Cl₂N₂O₂
Molecular Weight:299.156
Hs Code.:

Synonyms:1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester

Suppliers and Price of 1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
1-(2,6-Dichloro-phenyl)-5-methyl-1H-pyrazole-3-carboxylicacidethylester 95%+
1g
$ 690.00

Advanced Chemicals Intermediatesced Chemicals Intermediates
1-(2,6-Dichloro-phenyl)-5-methyl-1H-pyrazole-3-carboxylicacidethylester 95%+
5g
$ 978.75

Advanced Chemicals Intermediatesced Chemicals Intermediates
1-(2,6-Dichloro-phenyl)-5-methyl-1H-pyrazole-3-carboxylicacidethylester 95%+
10g
$ 1732.75

Acints
1-(2,6-Dichloro-phenyl)-5-methyl-1H-pyrazole-3-carboxylicacidethylester 95%+
10g
$ 1732.75

Acints
1-(2,6-Dichloro-phenyl)-5-methyl-1H-pyrazole-3-carboxylicacidethylester 95%+
5g
$ 978.75

Acints
1-(2,6-Dichloro-phenyl)-5-methyl-1H-pyrazole-3-carboxylicacidethylester 95%+
1g
$ 282.75

Total 2 raw suppliers

Chemical Property of 1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

1-(2,6-Dichloro-phenyl)-5-methyl-1H-pyrazole-3-carboxylicacidethylester 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester

There total 1 articles about 1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 615-79-2
ethyl 2,4-diketopentanoate

: 14763-24-7
(2,6-dichlorophenyl)hydrazine

: 1033586-29-6
1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester

Guidance literature:: ethyl 2,4-diketopentanoate; (2,6-dichlorophenyl)hydrazine; In ethanol; acetic acid; at 80 ℃; for 18h;

With sodium hydroxide; In ethanol; water; ethyl acetate;

Reference yield: 38.0%

: 1033586-29-6
1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester

: 1033586-30-9
5-bromomethyl-1-(2,6-dichlorophenyl)-1H-pyrazole-3-carboxylic acid ethyl ester

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 2h; Heating / reflux; high intensity lamp;

Reference yield:

: 1033586-29-6
1-(2,6-dichlorophenyl)-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester

: 1033575-52-8
2-chloro-4'-[2-(2,6-dichlorophenyl)-5-isopropyl-2H-pyrazol-3-ylmethoxy]biphenyl-4-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 2 h / Heating / reflux; high intensity lamp

2: potassium carbonate / acetonitrile / 4 h / Heating / reflux

3: tetrahydrofuran / 1.17 h / 0 - 20 °C

4: triethylsilane; trifluoroacetic acid / 1 h

5: water; potassium carbonate / (1,1'-bis(diphenylphosphine)ferrocene)palladium⁽⁰⁾ / 1,2-dimethoxyethane / 4 h / 80 °C

With triethylsilane; N-Bromosuccinimide; water; potassium carbonate; trifluoroacetic acid; dibenzoyl peroxide; (1,1'-bis(diphenylphosphine)ferrocene)palladium⁽⁰⁾; In tetrahydrofuran; tetrachloromethane; 1,2-dimethoxyethane; acetonitrile; 5: Suzuki Coupling;