C₈H₁₃(CH₂OCH₃)B(OCH₃)

Base Information

Chemical Name:C₈H₁₃(CH₂OCH₃)B(OCH₃)
CAS No.:74789-87-0
Molecular Formula:C₁₁H₂₁BO₂
Molecular Weight:196.098
Hs Code.:

C<sub>8</sub>H<sub>13</sub>(CH<sub>2</sub>OCH<sub>3</sub>)B(OCH<sub>3</sub>)

Synonyms:C₈H₁₃(CH₂OCH₃)B(OCH₃)

Suppliers and Price of C₈H₁₃(CH₂OCH₃)B(OCH₃)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of C₈H₁₃(CH₂OCH₃)B(OCH₃)

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of C₈H₁₃(CH₂OCH₃)B(OCH₃)

There total 3 articles about C₈H₁₃(CH₂OCH₃)B(OCH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 74789-86-9
3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

: 124-41-4
sodium methylate

: 74789-87-0
C₈H₁₃(CH₂OCH₃)B(OCH₃)

: 7647-15-6
sodium bromide

Guidance literature:: In methanol; (dry Ar); heated for 1.5 h at 50°C; MeOH vac. distd.; residue treated isopentane; ppt. NaBr filtered; filtrate distn.; elem. anal.;
DOI:10.1007/BF00949692

Reference yield: 42.0%

: 74789-86-9
3-methoxy-7-bromomethyl-3-borabicyclo[3.3.1]nonane

: 109-89-7
diethylamine

: 39238-98-7
3-methoxy-7-methylene-3-borabicyclo{3.3.1.}nonane

: 74789-87-0
C₈H₁₃(CH₂OCH₃)B(OCH₃)

: 74789-89-2
3-methoxy-7-diethylaminomethyl-3-borabicyclo[3.3.1]nonane*HCl

: 6274-12-0
diethylamine hydrobromide

Guidance literature:: With hydrogenchloride; In diethylamine; (dry Ar); heated in sealed ampul for 80 h at 100°C; ppt. Et2NH*HBr filtered; filtrate treated MeOH; fraction vac. distn.; treated ether soln. HCl; sepd.; filtrate distn.; elem. anal.;
DOI:10.1007/BF00949692

Reference yield: 30.0%

: 61357-36-6
1-boraadamantane tetrahydrofuranate

: 865-34-9
lithium methanolate

: 74789-87-0
C₈H₁₃(CH₂OCH₃)B(OCH₃)

: dimethoxy[3,5-di(iodomethyl)cyclohex-1-ylmethyl]borane

: dimethoxy(3-iodomethyl-5-methoxymethylcyclohex-1-ylmethyl)borane

: 128315-94-6
3-methoxy-7α-iodomethyl-3-borabicyclo<3.3.1>nonane

Guidance literature:: With iodine; In tetrahydrofuran; methanol; under Ar, to ate complex (from THF complex in THF and MeOLi in MeOH) added dropwise at -30°C soln. of I2 in THF, heated to 20°C, cooled to -30°C, subsequently added MeOLi and I2 in THF, heated to 20°C; evapd., MeOH added, extd. with hexane, treated with Na2S2O3*5H2O, evapd., fractionally distd.; elem. anal.;
DOI:10.1016/S0022-328X(00)98647-9