silyl>(trimethylsilyl)diazomethan

Base Information

• Chemical Name: silyl>(trimethylsilyl)diazomethan
• CAS No.: 108148-89-6
• Molecular Formula: C₁₃H₃₃N₃Si₃
• Molecular Weight: 315.682

Synonyms:silyl>(trimethylsilyl)diazomethan

Chemical Property of silyl>(trimethylsilyl)diazomethan

Chemical Property:

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Technology Process of silyl>(trimethylsilyl)diazomethan

There total 2 articles about silyl>(trimethylsilyl)diazomethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butyl azide (13686-33-4) + 4,4a-dihydro-3,3-dimethyl-1-phenyl-4,4-bis(trimethylsilyl)-3H-2-oxa-3-silanaphthaline (80431-42-1) → benzophenone (119-61-9) + silyl>(trimethylsilyl)diazomethan (108148-89-6) + 3-tert-Butyl-4,4-dimethyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-sila-1-cyclopenten (108148-83-0)

Guidance literature:

In benzene; at 90 ℃; for 3h; Rate constant; half live time;

Reference yield:

t-butyl azide (13686-33-4) + 2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan (80431-36-3) → diphenylmethyleneaminotrimethylsilane (17599-59-6) + silyl>(trimethylsilyl)diazomethan (108148-89-6)

Guidance literature:

In diethyl ether; at 100 ℃; for 12h;

upstream raw materials:

t-butyl azide

2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan

4,4a-dihydro-3,3-dimethyl-1-phenyl-4,4-bis(trimethylsilyl)-3H-2-oxa-3-silanaphthaline

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