2-{(4R,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}ethylamine

Base Information

Chemical Name:2-{(4R,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}ethylamine
CAS No.:1262052-10-7
Molecular Formula:C₁₇H₂₇NO₃
Molecular Weight:293.406
Hs Code.:

Synonyms:2-{(4R,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}ethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-{(4R,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}ethylamine

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Technology Process of 2-{(4R,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}ethylamine

There total 17 articles about 2-{(4R,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1262052-09-4
(4R,6S)-4-(2-azidoethyl)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxane

: 1262052-10-7
2-{(4R,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}ethylamine

Guidance literature:: With water; triphenylphosphine; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.tet.2010.10.028

Reference yield: 80.0%

: (4S,6R)-4-(2-benzyloxy-ethyl)-2,2-dimethyl-6-(2-nitro-ethyl)-1,3-dioxane

: 1262052-10-7
2-{(4R,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}ethylamine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 25 ℃; under 760.051 Torr;

Reference yield: 72.0%

: 1431291-03-0
2-{(4S,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}acetamide

: 1262052-10-7
2-{(4R,6S)-6-[2-(benzyloxy)ethyl]-2,2-dimethyl-1,3-dioxan-4-yl}ethylamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 12h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201201154