C₂₀H₂₂BrNO₃

Base Information

Chemical Name:C₂₀H₂₂BrNO₃
CAS No.:1383028-90-7
Molecular Formula:C₂₀H₂₂BrNO₃
Molecular Weight:404.304
Hs Code.:

C<sub>20</sub>H<sub>22</sub>BrNO<sub>3</sub>

Synonyms:C₂₀H₂₂BrNO₃

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Chemical Property of C₂₀H₂₂BrNO₃

Chemical Property:

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Technology Process of C₂₀H₂₂BrNO₃

There total 4 articles about C₂₀H₂₂BrNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 676627-65-9
C₁₁H₁₄BrNO₂

: 103-80-0
phenylacetyl chloride

: 1383028-90-7
C₂₀H₂₂BrNO₃

Guidance literature:: methanol; C₁₁H₁₄BrNO₂; With thionyl chloride; Reflux;

phenylacetyl chloride; With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 101184-73-0
2-(4-bromophenyl)-2-methylpropanenitrile

: 1383028-90-7
C₂₀H₂₂BrNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / dichloromethane / 1.5 h / -78 °C

1.2: 20 °C

2.1: sodium cyanide / water / Reflux

3.1: sodium hydroxide; water / ethylene glycol / 38 h / 120 °C

3.2: 20 °C

4.1: thionyl chloride / Reflux

4.2: 0.5 h / 0 °C

With sodium cyanide; thionyl chloride; water; diisobutylaluminium hydride; sodium hydroxide; In dichloromethane; water; ethylene glycol;

Reference yield:

: 32454-16-3
2-(4-bromophenyl)-2-methyl-propionaldehyde

: 1383028-90-7
C₂₀H₂₂BrNO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium cyanide / water / Reflux

2.1: sodium hydroxide; water / ethylene glycol / 38 h / 120 °C

2.2: 20 °C

3.1: thionyl chloride / Reflux

3.2: 0.5 h / 0 °C

With sodium cyanide; thionyl chloride; water; sodium hydroxide; In water; ethylene glycol;