N-(5-(2-(4-(4-hydroxybutyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

Base Information

• Chemical Name: N-(5-(2-(4-(4-hydroxybutyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide
• CAS No.: 896472-84-7
• Molecular Formula: C₂₀H₃₁NO₄
• Molecular Weight: 349.47

Synonyms:N-(5-(2-(4-(4-hydroxybutyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

Chemical Property of N-(5-(2-(4-(4-hydroxybutyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

Chemical Property:

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Technology Process of N-(5-(2-(4-(4-hydroxybutyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

There total 2 articles about N-(5-(2-(4-(4-hydroxybutyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

ethyl 4-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)butanoate (896472-83-6) → N-(5-(2-(4-(4-hydroxybutyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide (896472-84-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1016/S0960-894X(99)00695-2

Reference yield: 50.0%

2,2-dimethoxy-propane (77-76-9) + diethyl 2-acetylamino-2-(2-(4-(3-ethoxycarbonylpropyl)phenyl)ethyl)propane-1,3-dioate (896472-82-5) → N-(5-(2-(4-(4-hydroxybutyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide (896472-84-7) + ethyl 4-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)butanoate (896472-83-6)

Guidance literature:

diethyl 2-acetylamino-2-(2-(4-(3-ethoxycarbonylpropyl)phenyl)ethyl)propane-1,3-dioate; With sodium tetrahydroborate; In methanol;

2,2-dimethoxy-propane; With toluene-4-sulfonic acid;

DOI:10.1016/S0960-894X(99)00695-2

Reference yield: 93.0%

N-(5-(2-(4-(4-hydroxybutyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide (896472-84-7) → N-(2,2-dimethyl-5-(2-(4-(4-oxobutyl)phenyl)ethyl)-1,3-dioxan-5-yl)ethanamide (896472-85-8)

Guidance literature:

With oxalyl dichloride; In dichloromethane; dimethyl sulfoxide; at -70 ℃; for 0.166667h;

DOI:10.1016/j.bmc.2006.01.071

upstream raw materials:

2,2-dimethoxy-propane

diethyl 2-acetylamino-2-(2-(4-(3-ethoxycarbonylpropyl)phenyl)ethyl)propane-1,3-dioate

ethyl 4-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)butanoate

Downstream raw materials:

4-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)butyl 4-methylbenzenesulfonate

N-(2,2-dimethyl-5-(2-(4-(4-oxobutyl)phenyl)ethyl)-1,3-dioxan-5-yl)ethanamide

N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate

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