N,N-DIETHYL CHLOROFLUOROACETAMIDE

Base Information

• Chemical Name: N,N-DIETHYL CHLOROFLUOROACETAMIDE
• CAS No.: 364-94-3
• Molecular Formula: C6H11ClFNO
• Molecular Weight: 167.611
• Hs Code.: 2924199090
• Mol file: 364-94-3.mol

Synonyms:2-Chloro-N,N-diethyl-2-fluoroacetamide;N,N-Diethyl chlorofluoroacetamide;N1,N1-Diethyl-2-chloro-2-fluoroacetamide;

Chemical Property of N,N-DIETHYL CHLOROFLUOROACETAMIDE

Chemical Property:

• Vapor Pressure: 0.197mmHg at 25°C
• Refractive Index: 1.43
• Boiling Point: 210 °C at 760 mmHg
• Flash Point: 80.8 °C
• PSA: 20.31000
• Density: 1.123 g/cm³
• LogP: 1.38920

Purity/Quality:

98%Min ^*data from raw suppliers

N,N-DiethylChlorofluoroacetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-DIETHYL CHLOROFLUOROACETAMIDE

There total 4 articles about N,N-DIETHYL CHLOROFLUOROACETAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-chloro-1,1,2-trifluoroethyl)diethylamine (357-83-5) + pentachloro-2-(trimethylsiloxy)propene (87651-34-1) → trimethylsilyl fluoride (420-56-4) + N,N-diethylchlorofluoroacetamide (364-94-3) + 2-fluoropentachloropropylene (815-15-6)

Guidance literature:

at 80 ℃; for 2h;

Reference yield:

N-(2-chloro-1,1,2-trifluoroethyl)diethylamine (357-83-5) + butan-1-ol (71-36-3) → 1-fluorobutane (2366-52-1) + N,N-diethylchlorofluoroacetamide (364-94-3)

Guidance literature:

Reference yield:

2,2-dichloro-1,1-difluoroethyldiethylamine (67406-60-4) → N,N-diethyl-2,2-difluoroacetamide (686-11-3) + N,N-diethylchlorofluoroacetamide (364-94-3) + N,N-diethyldichloroacetamide (921-88-0)

Guidance literature:

With water; triethylamine; In dimethyl sulfoxide; for 28h; Product distribution; other solvent, other time.;

upstream raw materials:

N-(2-chloro-1,1,2-trifluoroethyl)diethylamine

butan-1-ol

pentachloro-2-(trimethylsiloxy)propene

2,2-dichloro-1,1-difluoroethyldiethylamine

Refernces

• 1、 Kukhar', V. P.,Migaichuk, I. V.,Lazukina, L. A.,Trikhleb, L. M.,Khaskin, I. G.. "PENTACHLORO-2-(TRIMETHYLSILOXY)PROPENE". . p. 1424 - 1427. Retrieved 2007/10/02.