C₂₀H₂₉FN₂O₄

Base Information

Chemical Name:C₂₀H₂₉FN₂O₄
CAS No.:1014703-33-3
Molecular Formula:C₂₀H₂₉FN₂O₄
Molecular Weight:380.46
Hs Code.:

C<sub>20</sub>H<sub>29</sub>FN<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₀H₂₉FN₂O₄

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Chemical Property of C₂₀H₂₉FN₂O₄

Chemical Property:

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Technology Process of C₂₀H₂₉FN₂O₄

There total 8 articles about C₂₀H₂₉FN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 644982-65-0
[1-{[(1,1-dimethylethyl)oxy]carbonyl}-4-(3-fluorophenyl)-4-piperidinyl]acetic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1014703-33-3
C₂₀H₂₉FN₂O₄

Guidance literature:: [1-{[(1,1-dimethylethyl)oxy]carbonyl}-4-(3-fluorophenyl)-4-piperidinyl]acetic acid; N,O-dimethylhydroxylamine*hydrochloride; With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 20 ℃;

With sodium hydroxide; In dichloromethane; water; for 0.166667h;

Reference yield:

: 193537-11-0
tert-butyl 4-(1-cyano-2-ethoxy-2-oxoethylidene)-4-piperidine-1-carboxylate

: 1014703-33-3
C₂₀H₂₉FN₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(l) iodide / tetrahydrofuran / 3 h / 0 °C

2.1: sodium hydroxide / ethanol; water / 15 h / 20 °C

2.2: 0 °C / pH 3

3.1: copper(I) oxide / acetonitrile / 1 - 1.25 h / Heating / reflux

4.1: diisobutylaluminium hydride / dichloromethane / 4 h / -78 - -60 °C

5.1: sodium hypochlorite; sodium carbonate / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 20 °C

6.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 20 °C

6.2: 0.17 h

With copper(I) oxide; sodium hydroxide; sodium hypochlorite; diisobutylaluminium hydride; sodium carbonate; N-ethyl-N,N-diisopropylamine; HATU; copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 878130-44-0
4-(3-fluoro-phenyl)-4-(2-oxo-ethyl)-piperidine-1-carboxylic acid tert-butyl ester

: 1014703-33-3
C₂₀H₂₉FN₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hypochlorite; sodium carbonate / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 20 °C

2.2: 0.17 h

With sodium hypochlorite; sodium carbonate; N-ethyl-N,N-diisopropylamine; HATU; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In dichloromethane; water;