5-chloro-2-nitro-N-(1-(3-(trifluoromethyl)phenyl)-1H-pyrazol-3-yl)-benzamide

Base Information

Chemical Name:5-chloro-2-nitro-N-(1-(3-(trifluoromethyl)phenyl)-1H-pyrazol-3-yl)-benzamide
CAS No.:1354722-15-8
Molecular Formula:C₁₇H₁₀ClF₃N₄O₃
Molecular Weight:410.74
Hs Code.:

Synonyms:5-chloro-2-nitro-N-(1-(3-(trifluoromethyl)phenyl)-1H-pyrazol-3-yl)-benzamide

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Chemical Property of 5-chloro-2-nitro-N-(1-(3-(trifluoromethyl)phenyl)-1H-pyrazol-3-yl)-benzamide

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Technology Process of 5-chloro-2-nitro-N-(1-(3-(trifluoromethyl)phenyl)-1H-pyrazol-3-yl)-benzamide

There total 3 articles about 5-chloro-2-nitro-N-(1-(3-(trifluoromethyl)phenyl)-1H-pyrazol-3-yl)-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 41994-44-9
5-chloro-2-nitrobenzoyl chloride

: 66000-41-7
1-(3-(trifluoromethyl)phenyl)-3-amino-1H-pyrazole

: 1354722-15-8
5-chloro-2-nitro-N-(1-(3-(trifluoromethyl)phenyl)-1H-pyrazol-3-yl)-benzamide

Guidance literature:: With pyridine; at 20 ℃; for 1h;

Reference yield:

: 401-81-0
m-trifluoromethylphenyl iodide

: 1354722-15-8
5-chloro-2-nitro-N-(1-(3-(trifluoromethyl)phenyl)-1H-pyrazol-3-yl)-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; L-proline; copper(l) iodide / dimethyl sulfoxide / 85 °C

2: hydrogen / palladium on activated charcoal / methanol / 20 °C

3: pyridine / 1 h / 20 °C

With pyridine; copper(l) iodide; hydrogen; potassium carbonate; L-proline; palladium on activated charcoal; In methanol; dimethyl sulfoxide;

Reference yield:

: 1354722-12-5
3-nitro-1-(3-(trifluoromethyl)phenyl)-1H-pyrazole

: 1354722-15-8
5-chloro-2-nitro-N-(1-(3-(trifluoromethyl)phenyl)-1H-pyrazol-3-yl)-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium on activated charcoal / methanol / 20 °C

2: pyridine / 1 h / 20 °C

With pyridine; hydrogen; palladium on activated charcoal; In methanol;