2,3-Dichlorobenzamide

Base Information

• Chemical Name: 2,3-Dichlorobenzamide
• CAS No.: 5980-24-5
• Molecular Formula: C7H5Cl2NO
• Molecular Weight: 190.029
• Hs Code.: 2924299090
• DSSTox Substance ID: DTXSID00371045
• Wikidata: Q82158265
• Mol file: 5980-24-5.mol

Synonyms:2,3-Dichlorobenzamide;5980-24-5;2,3-dichloro-benzamide;dichlorobenzamide;Benzamide, 2,3-dichloro-;2,3-bis(chloranyl)benzamide;SCHEMBL112377;NIOSH/CV3459562;DTXSID00371045;KZKYRHRAVGWEAV-UHFFFAOYSA-N;MFCD00173938;AKOS008937417;AS-57607;LS-26321;CS-0207354;CV34595620;FT-0609552;E83825;A832475

Chemical Property of 2,3-Dichlorobenzamide

Chemical Property:

• Vapor Pressure: 0.0107mmHg at 25°C
• Melting Point: 170-172 °C
• Refractive Index: 1.596
• Boiling Point: 268 °C at 760 mmHg
• PKA: 14.77±0.50(Predicted)
• Flash Point: 115.9 °C
• PSA: 43.09000
• Density: 1.439 g/cm³
• LogP: 2.79260
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 188.9748192
• Heavy Atom Count: 11
• Complexity: 163

Purity/Quality:

98%min ^*data from raw suppliers

2,3-Dichlorobenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: R36/37/38:
• Safety Statements: S26:

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C(=C1)Cl)Cl)C(=O)N

Technology Process of 2,3-Dichlorobenzamide

There total 7 articles about 2,3-Dichlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

2,3-dichlorbenzoic acid (50-45-3) + urea (57-13-6) → 2,3-dichlorobenzamide (5980-24-5)

Guidance literature:

With formic acid; at 130 - 180 ℃; for 2h;

DOI:10.1007/BF02218429

Reference yield:

2,3-dichlorobenzoyl chloride (2905-60-4) → 2,3-dichlorobenzamide (5980-24-5)

Guidance literature:

With ammonium hydroxide; In ethyl acetate;

DOI:10.1021/jm990567u

Reference yield:

oxalyl dichloride (79-37-8) + 2,3-dichlorbenzoic acid (50-45-3) → 2,3-dichlorobenzamide (5980-24-5)

Guidance literature:

In toluene;

upstream raw materials:

2,3-dichlorbenzoic acid

urea

2,3-dichlorobenzonitrile

2,3-dichlorobenzoyl chloride

Downstream raw materials:

2,3-dichloro-N-[(dimethylamino)methylene]benzamide

2,3-dichlorobenzothioamide

ethyl 2,3-dichlorobenzimidate

2,3-dichlorobenzoyl chloride