2-hydroxy-3-nitro-5-(2-oxo-5,6-diphenyl-1,2,3,4-tetrahydropyrimidin-4-yl)benzonitrile

Base Information

Chemical Name:2-hydroxy-3-nitro-5-(2-oxo-5,6-diphenyl-1,2,3,4-tetrahydropyrimidin-4-yl)benzonitrile
CAS No.:1283118-52-4
Molecular Formula:C₂₃H₁₆N₄O₄
Molecular Weight:412.404
Hs Code.:

Synonyms:2-hydroxy-3-nitro-5-(2-oxo-5,6-diphenyl-1,2,3,4-tetrahydropyrimidin-4-yl)benzonitrile

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Chemical Property of 2-hydroxy-3-nitro-5-(2-oxo-5,6-diphenyl-1,2,3,4-tetrahydropyrimidin-4-yl)benzonitrile

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Technology Process of 2-hydroxy-3-nitro-5-(2-oxo-5,6-diphenyl-1,2,3,4-tetrahydropyrimidin-4-yl)benzonitrile

There total 4 articles about 2-hydroxy-3-nitro-5-(2-oxo-5,6-diphenyl-1,2,3,4-tetrahydropyrimidin-4-yl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 451-40-1
phenyl benzyl ketone

: 1283118-53-5
5-formyl-2-hydroxy-3-nitrobenzonitrile

: 57-13-6
urea

: 1283118-52-4
2-hydroxy-3-nitro-5-(2-oxo-5,6-diphenyl-1,2,3,4-tetrahydropyrimidin-4-yl)benzonitrile

Guidance literature:: With hydrogenchloride; In ethanol; water; for 37h; Reflux;

Reference yield:

: 2973-78-6
3-bromo-4-hydroxybenzylaldehyde

: 1283118-52-4
2-hydroxy-3-nitro-5-(2-oxo-5,6-diphenyl-1,2,3,4-tetrahydropyrimidin-4-yl)benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 8 h / 180 °C

2: nitric acid; acetic acid / 5 h / 0 °C

3: hydrogenchloride / ethanol; water / 37 h / Reflux

With hydrogenchloride; nitric acid; acetic acid; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 611-20-1
salicylonitrile

: 1283118-52-4
2-hydroxy-3-nitro-5-(2-oxo-5,6-diphenyl-1,2,3,4-tetrahydropyrimidin-4-yl)benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 2 h / 120 °C

2: nitric acid; acetic acid / 5 h / 0 °C

3: hydrogenchloride / ethanol; water / 37 h / Reflux

With hydrogenchloride; nitric acid; acetic acid; In ethanol; water;