ethyl bis(4-chlorophenyl)phosphinate

Base Information

Chemical Name:ethyl bis(4-chlorophenyl)phosphinate
CAS No.:114617-83-3
Molecular Formula:C₁₄H₁₃Cl₂O₂P
Molecular Weight:315.136
Hs Code.:

Synonyms:ethyl bis(4-chlorophenyl)phosphinate

Suppliers and Price of ethyl bis(4-chlorophenyl)phosphinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl bis(4-chlorophenyl)phosphinate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl bis(4-chlorophenyl)phosphinate

There total 3 articles about ethyl bis(4-chlorophenyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 64-17-5
ethanol

: 15948-60-4
bis(4-chlorophenyl)phosphine oxide

: 114617-83-3
ethyl bis(4-chlorophenyl)phosphinate

Guidance literature:: With Selectfluor; In acetonitrile; at 60 ℃; for 12h;
DOI:10.1021/acs.joc.6b01932

Reference yield:

: 108-90-7
chlorobenzene

: 2373-43-5
diethyl (4-chlorophenyl)phosphonate

: 114617-83-3
ethyl bis(4-chlorophenyl)phosphinate

Guidance literature:: With aluminium trichloride; phosphorus trichloride; Einleiten von Chlor in eine Loesung des Reaktionsprodukts in 1.1.2.2-Tetrachlor-aethan und anschliessenden Behandeln mit Aethanol;
DOI:10.1021/ja01200a059

Reference yield:

: 7446-70-0
aluminium trichloride

: 108-90-7
chlorobenzene

: 7719-12-2,52843-90-0
phosphorus trichloride

: 2373-43-5
diethyl (4-chlorophenyl)phosphonate

: 114617-83-3
ethyl bis(4-chlorophenyl)phosphinate

Guidance literature:: Behandlung des in Tetrachloraethan geloesten Reaktionsprodukts mit Chlor und anschliessende Veresterung mit Aethanol bei 15grad;
DOI:10.1021/ja01200a059