[7,7'-(1,3-phenylenebis(methylene))bis[1,5-diphenyl-3-(1,4,6-trimethyl-1,4-diazepan-6-yl)-3,7-diazabicyclo[3.3.1]nonan-9-one]]

Base Information

Chemical Name:[7,7'-(1,3-phenylenebis(methylene))bis[1,5-diphenyl-3-(1,4,6-trimethyl-1,4-diazepan-6-yl)-3,7-diazabicyclo[3.3.1]nonan-9-one]]
CAS No.:1359849-53-8
Molecular Formula:C₆₂H₇₈N₈O₂
Molecular Weight:967.354
Hs Code.:

Synonyms:[7,7'-(1,3-phenylenebis(methylene))bis[1,5-diphenyl-3-(1,4,6-trimethyl-1,4-diazepan-6-yl)-3,7-diazabicyclo[3.3.1]nonan-9-one]]

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Chemical Property of [7,7'-(1,3-phenylenebis(methylene))bis[1,5-diphenyl-3-(1,4,6-trimethyl-1,4-diazepan-6-yl)-3,7-diazabicyclo[3.3.1]nonan-9-one]]

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Technology Process of [7,7'-(1,3-phenylenebis(methylene))bis[1,5-diphenyl-3-(1,4,6-trimethyl-1,4-diazepan-6-yl)-3,7-diazabicyclo[3.3.1]nonan-9-one]]

There total 1 articles about [7,7'-(1,3-phenylenebis(methylene))bis[1,5-diphenyl-3-(1,4,6-trimethyl-1,4-diazepan-6-yl)-3,7-diazabicyclo[3.3.1]nonan-9-one]] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1477-55-0
1,3-di(aminomethyl)benzene

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1101929-26-3
1-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)-3,5-diphenylpiperidine-4-one

: 1359849-53-8
[7,7'-(1,3-phenylenebis(methylene))bis[1,5-diphenyl-3-(1,4,6-trimethyl-1,4-diazepan-6-yl)-3,7-diazabicyclo[3.3.1]nonan-9-one]]

Guidance literature:: With acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; at 80 ℃; for 12h;
DOI:10.1021/ic2019296

Reference yield: 73.0%

: 425370-02-1
tetrakis(acetonitrile)copper(I) tetrakis(pentafluorophenyl)borate

: 1359849-53-8
[7,7'-(1,3-phenylenebis(methylene))bis[1,5-diphenyl-3-(1,4,6-trimethyl-1,4-diazepan-6-yl)-3,7-diazabicyclo[3.3.1]nonan-9-one]]

: Cu⁽²⁺⁾*(C₂H₄N₂(CH₃)2C₂H₄CCH₃NC₂H₄C₂COC₂H₄N(C₆H₅)2)2CH₂C₆H₄CH₂*2B(C₆F₅)4^(1-)=CuC₆₂H₇₈N₈O₂(B(C₆F₅)4)2

Guidance literature:: In tetrahydrofuran; acetonitrile; a soln. of Cu-complex and aza-compound in deoxygenated THF with 3 drops of CH3CN was stirred for 30 min under an oxygen-free atm.; deoxygenated pentane was aded, the solvent was removed in vac.;
DOI:10.1021/ic2019296

Reference yield: 73.0%

: 67-56-1
methanol

: hexaaquocopper(II) tetrafluoroborate

: 1359849-53-8
[7,7'-(1,3-phenylenebis(methylene))bis[1,5-diphenyl-3-(1,4,6-trimethyl-1,4-diazepan-6-yl)-3,7-diazabicyclo[3.3.1]nonan-9-one]]

: 2Cu⁽²⁺⁾*(C₂H₄N₂(CH₃)2C₂H₄CCH₃NC₂H₄C₂COC₂H₄N(C₆H₅)2)2CH₂C₆H₄CH₂*2BF₄^(1-)*2F^(1-)*2CH₃OH=Cu₂C₆₂H₇₈N₈O₂(BF₄)2F₂*2CH₃OH

Guidance literature:: In acetonitrile; a soln. of Cu-complex in CH3CN was added to a soln. of aza-compound in CH3CN, stirred at ambient temp. overnight; treated with a diethyl ether diffusion, pptn. with CH3OH; elem. anal.;
DOI:10.1021/ic2019296