4,4-dimethyl-1-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}semicarbazide

Base Information

Chemical Name:4,4-dimethyl-1-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}semicarbazide
CAS No.:1237587-35-7
Molecular Formula:C₁₉H₁₆Cl₃F₃N₄O₂
Molecular Weight:495.716
Hs Code.:

Synonyms:4,4-dimethyl-1-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}semicarbazide

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Chemical Property of 4,4-dimethyl-1-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}semicarbazide

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Technology Process of 4,4-dimethyl-1-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}semicarbazide

There total 6 articles about 4,4-dimethyl-1-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}semicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237587-85-7
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenylhydrazine

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 1237587-35-7
4,4-dimethyl-1-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}semicarbazide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 1237587-35-7
4,4-dimethyl-1-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}semicarbazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid / iron / ethanol / 0.83 h / 75 °C

3.1: hydrogenchloride / 1,4-dioxane; water / 0.33 h / 20 °C

3.2: 0.25 h / 0 °C

4.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

With hydrogenchloride; N-chloro-succinimide; water; acetic acid; triethylamine; iron; In tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 66399-01-7
2-chloro-5-hydroxyiminomethylnitrobenzene

: 1237587-35-7
4,4-dimethyl-1-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-chlorophenyl}semicarbazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid / iron / ethanol / 0.83 h / 75 °C

3.1: hydrogenchloride / 1,4-dioxane; water / 0.33 h / 20 °C

3.2: 0.25 h / 0 °C

4.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

With hydrogenchloride; N-chloro-succinimide; water; acetic acid; triethylamine; iron; In tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;