(2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate

Base Information

Chemical Name:(2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate
CAS No.:1555699-22-3
Molecular Formula:C₂HF₃O₂*C₁₄H₁₃F₃N₂O
Molecular Weight:396.289
Hs Code.:

Synonyms:(2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate

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Chemical Property of (2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate

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Technology Process of (2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate

There total 2 articles about (2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 1555699-22-3
(2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

1.2: 16 h / 20 °C

2.1: sodium nitrite; hydrogenchloride / water / 0.33 h / -10 - 0 °C

2.2: 1.33 h

With hydrogenchloride; potassium carbonate; sodium nitrite; In water; N,N-dimethyl-formamide;

Reference yield:

: 400-99-7
2-nitro-4-trifluoromethylphenol

: 1555699-22-3
(2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

1.2: 16 h / 20 °C

2.1: sodium nitrite; hydrogenchloride / water / 0.33 h / -10 - 0 °C

2.2: 1.33 h

With hydrogenchloride; potassium carbonate; sodium nitrite; In water; N,N-dimethyl-formamide;

Reference yield: 68.0%

: 1555699-22-3
(2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate

: 78-84-2
isobutyraldehyde

: 1555699-26-7
7-(benzyloxy)-3,3-dimethyl-4-(trifluoromethyl)indoline

Guidance literature:: (2-(benzyloxy)-5-(trifluoromethyl)phenyl)hydrazine trifluoroacetate; isobutyraldehyde; With sulfuric acid; In ethanol; at 0 - 20 ℃; for 24h;

With methanol; sodium tetrahydroborate; at 0 ℃; for 0.5h;