METHYL ALPHA-BROMO-2-CHLOROPHENYLACETATE

Base Information

• Chemical Name: METHYL ALPHA-BROMO-2-CHLOROPHENYLACETATE
• CAS No.: 115871-49-3
• Molecular Formula: C₉H₈BrClO₂
• Molecular Weight: 263.518
• Hs Code.: 29163990
• Mol file: 115871-49-3.mol

Synonyms:Methyl2-Bromo-2鈥ChlorophenylAcetate;Methyl α-bromo-2-chlorophenylacetate ,97%

Chemical Property of METHYL ALPHA-BROMO-2-CHLOROPHENYLACETATE

Chemical Property:

• Appearance/Colour: Light-Yellow Oil
• Refractive Index: 1.556
• Boiling Point: 281.096oC at 760 mmHg
• Flash Point: 123.802oC
• PSA: 26.30000
• Density: 1.546
• LogP: 2.81800

Purity/Quality:

99% ^*data from raw suppliers

Methyl2-bromo-4-chlorophenylacetate ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-37

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Methyl 2-bromo-4-chlorophenylacetate

Technology Process of METHYL ALPHA-BROMO-2-CHLOROPHENYLACETATE

There total 2 articles about METHYL ALPHA-BROMO-2-CHLOROPHENYLACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 2-(2-bromo-4-chlorophenyl)acetic acid (52864-56-9) → methyl 2-(2-bromo-4-chlorophenyl)acetate (115871-49-3)

Guidance literature:

With sulfuric acid; for 3h; Reflux;

DOI:10.1002/anie.201603576

Reference yield:

→ methyl 2-(2-bromo-4-chlorophenyl)acetate (115871-49-3) + 2,4-dibromophenylacetate methyl ester (66247-65-2)

Guidance literature:

Reference yield: 98.0%

N-Acetylimidazole (2466-76-4) + methyl 2-(2-bromo-4-chlorophenyl)acetate (115871-49-3) → methyl 2-(2-bromo-4-chlorophenyl)-3-hydroxybut-2-enoate

Guidance literature:

methyl 2-(2-bromo-4-chlorophenyl)acetate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

N-Acetylimidazole; In tetrahydrofuran; N,N-dimethyl acetamide; at -78 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ol5018118

upstream raw materials:

methanol

2-(2-bromo-4-chlorophenyl)acetic acid

Downstream raw materials:

methyl 1-benzyl-2-methyl-1H-indole-3-carboxylate

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