allylbenzyl methylphosphonate

Base Information

• Chemical Name: allylbenzyl methylphosphonate
• CAS No.: 479404-17-6
• Molecular Formula: C₁₁H₁₅O₃P
• Molecular Weight: 226.212
• Mol file: 479404-17-6.mol

Synonyms:allylbenzyl methylphosphonate

Chemical Property of allylbenzyl methylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of allylbenzyl methylphosphonate

There total 2 articles about allylbenzyl methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

Allyl acetate (591-87-7) + dibenzyl methylphosphonate (19236-58-9) → allylbenzyl methylphosphonate (479404-17-6)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jo026247r

Reference yield: 33.0%

methylphosphonic acid dichloroanhydride (676-97-1) + allyl alcohol (107-18-6) + benzyl alcohol (100-51-6,185532-71-2) → allylbenzyl methylphosphonate (479404-17-6)

Guidance literature:

methylphosphonic acid dichloroanhydride; benzyl alcohol; With pyridine;

allyl alcohol; at 0 ℃; Further stages.;

DOI:10.1021/jo026247r

Reference yield: 90.0%

2,3,5-tri-O-benzyl-L-xylono-1,4-lactone (134307-32-7) + allylbenzyl methylphosphonate (479404-17-6) → 1-(allylbenzylphosphinyl)-1-deoxy-3,4,6-tri-O-(benzyl)-D-fructofuranose

Guidance literature:

allylbenzyl methylphosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h;

2,3,5-tri-O-benzyl-L-xylono-1,4-lactone; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Further stages.;

DOI:10.1021/jo026247r

upstream raw materials:

Allyl acetate

dibenzyl methylphosphonate

methylphosphonic acid dichloroanhydride

allyl alcohol