5α-spirostan-3β,12β-diyl 3-acetate 12-benzoate

Base Information Edit

Chemical Name:5α-spirostan-3β,12β-diyl 3-acetate 12-benzoate
CAS No.:21170-15-0
Molecular Formula:C₃₆H₅₀O₆
Molecular Weight:578.789
Hs Code.:
Mol file:21170-15-0.mol

Synonyms:5α-spirostan-3β,12β-diyl 3-acetate 12-benzoate

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Chemical Property of 5α-spirostan-3β,12β-diyl 3-acetate 12-benzoate Edit

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Technology Process of 5α-spirostan-3β,12β-diyl 3-acetate 12-benzoate

There total 2 articles about 5α-spirostan-3β,12β-diyl 3-acetate 12-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 98-88-4
benzoyl chloride

: 863-85-4
3β-acetoxy-12β-hydroxy-5α,25R-spirostan

: 21170-15-0
5α-spirostan-3β,12β-diyl 3-acetate 12-benzoate

Guidance literature:: With pyridine; dmap; at 25 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol2017033

Reference yield:

: 915-35-5
hecogenin acetate

: 21170-15-0
5α-spirostan-3β,12β-diyl 3-acetate 12-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: platinum; acetic acid; ethyl acetate / Hydrogenation

2: pyridine; benzene

With pyridine; acetic acid; ethyl acetate; platinum; benzene;
DOI:10.1021/ja01116a002