Technology Process of 3-acetamido-2,5-dimethoxy-2-(nitrobenzoyl)-acetanilide
There total 6 articles about 3-acetamido-2,5-dimethoxy-2-(nitrobenzoyl)-acetanilide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 21 g / glacial acetic acid; nitric acid / 15 - 30 °C
2: 99 percent / diethyl ether
3: cyclohexene / palladium on carbon / ethanol / 0.25 h / Heating
4: 6.5 g / acetic acid / 0.08 h / Heating
5: cyclohexene / palladium on carbon / ethanol / 24 h / Heating
6: 21 g / xylene / 2 h / 160 - 180 °C
With
nitric acid; acetic acid; cyclohexene;
palladium on activated charcoal;
In
diethyl ether; ethanol; xylene;
DOI:10.1021/jo7017813
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / diethyl ether
2: cyclohexene / palladium on carbon / ethanol / 0.25 h / Heating
3: 6.5 g / acetic acid / 0.08 h / Heating
4: cyclohexene / palladium on carbon / ethanol / 24 h / Heating
5: 21 g / xylene / 2 h / 160 - 180 °C
With
acetic acid; cyclohexene;
palladium on activated charcoal;
In
diethyl ether; ethanol; xylene;
DOI:10.1021/jo7017813
- Guidance literature:
-
Multi-step reaction with 4 steps
1: cyclohexene / palladium on carbon / ethanol / 0.25 h / Heating
2: 6.5 g / acetic acid / 0.08 h / Heating
3: cyclohexene / palladium on carbon / ethanol / 24 h / Heating
4: 21 g / xylene / 2 h / 160 - 180 °C
With
acetic acid; cyclohexene;
palladium on activated charcoal;
In
ethanol; xylene;
DOI:10.1021/jo7017813
