C₂₂H₂₃ClFNO₃

Base Information

Chemical Name:C₂₂H₂₃ClFNO₃
CAS No.:1344689-14-0
Molecular Formula:C₂₂H₂₃ClFNO₃
Molecular Weight:403.881
Hs Code.:

C<sub>22</sub>H<sub>23</sub>ClFNO<sub>3</sub>

Synonyms:C₂₂H₂₃ClFNO₃

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Chemical Property of C₂₂H₂₃ClFNO₃

Chemical Property:

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Technology Process of C₂₂H₂₃ClFNO₃

There total 11 articles about C₂₂H₂₃ClFNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₄FNO₄

: 1344689-14-0
C₂₂H₂₃ClFNO₃

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 93-17-4
3,4-dimethoxyphenylacetonitrile

: 1344689-14-0
C₂₂H₂₃ClFNO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: ethanol; sodium / toluene / 2 h / 80 - 85 °C

1.2: 2 h / 80 °C

2.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 2844.39 Torr

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 20 °C

4.1: phosphorus pentachloride / dichloromethane

5.1: sulfur / 0.33 h / 165 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 20 °C

7.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; ethanol; phosphorus pentachloride; hydrogen; sodium; benzotriazol-1-ol; sulfur; methanesulfonyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; toluene;

Reference yield:

: 36848-69-8
ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate

: 1344689-14-0
C₂₂H₂₃ClFNO₃

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 2844.39 Torr

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 20 °C

3: phosphorus pentachloride / dichloromethane

4: sulfur / 0.33 h / 165 °C

5: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 20 °C

6: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; phosphorus pentachloride; hydrogen; benzotriazol-1-ol; sulfur; methanesulfonyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water;