ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate

Base Information

Chemical Name:ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate
CAS No.:896472-86-9
Molecular Formula:C₂₆H₄₁NO₅
Molecular Weight:447.615
Hs Code.:

Synonyms:ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate

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Technology Process of ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate

There total 6 articles about ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)-2,4-octadienoate

: 896472-86-9
ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 2h;
DOI:10.1016/j.bmc.2006.01.071

Reference yield:

: 896472-85-8
N-(2,2-dimethyl-5-(2-(4-(4-oxobutyl)phenyl)ethyl)-1,3-dioxan-5-yl)ethanamide

: 896472-86-9
ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / sodium hydride / dimethylformamide / 0.5 h / -25 °C

2: 99 percent / hydrogen / Pd/C / ethyl acetate / 2 h

With hydrogen; sodium hydride; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide; 1: Wittig condensation;
DOI:10.1016/j.bmc.2006.01.071

Reference yield:

: 37746-78-4
4-bromo-trans-crotonic acid ethyl ester

: 896472-86-9
ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / benzene / 4 h / 20 °C

2: 52 percent / sodium hydride / dimethylformamide / 0.5 h / -25 °C

3: 99 percent / hydrogen / Pd/C / ethyl acetate / 2 h

With hydrogen; sodium hydride; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide; benzene; 2: Wittig condensation;
DOI:10.1016/j.bmc.2006.01.071