benzene

Base Information

• Chemical Name: benzene
• CAS No.: 132731-64-7
• Molecular Formula: C₁₆H₂₁IO₅S
• Molecular Weight: 452.31

Synonyms:benzene

Chemical Property of benzene

Chemical Property:

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Technology Process of benzene

There total 2 articles about benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

[bis(acetoxy)iodo]benzene (3240-34-4) + (1S)-10-camphorsulfonic acid (3144-16-9,61380-66-3) → benzene (132731-64-7)

Guidance literature:

With water; In acetonitrile; for 0.5h;

DOI:10.1021/jo00288a053

Reference yield: 80.0%

iodobenzene (591-50-4) + (1S)-10-camphorsulfonic acid (3144-16-9,61380-66-3) → benzene (132731-64-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 2h;

DOI:10.1055/s-2005-872697

Reference yield: 95.0%

benzene (132731-64-7) + acetophenone (98-86-2) → α-(camphorsulfonyloxy)acetophenone (87456-41-5)

Guidance literature:

In acetonitrile; at 80 ℃; for 0.25h;

DOI:10.1021/jo00288a053

upstream raw materials:

[bis(acetoxy)iodo]benzene

(1S)-10-camphorsulfonic acid

iodobenzene

Downstream raw materials:

α-(camphorsulfonyloxy)acetophenone

2-((10-camphorsulfonyl)oxy)-1-phenyl-1-propanone

iodobenzene

3-((10-camphorsulfonyl)oxy)-2-butanone

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