[Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2NC(O)Me)]

Base Information

Chemical Name:[Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2NC(O)Me)]
CAS No.:835633-34-6
Molecular Formula:C₂₃H₂₅N₂OPPd
Molecular Weight:482.858
Hs Code.:

Synonyms:[Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2NC(O)Me)]

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Chemical Property of [Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2NC(O)Me)]

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Technology Process of [Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2NC(O)Me)]

There total 1 articles about [Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2NC(O)Me)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: bis[(benzyldimethylamino)chloropalladium(II)]

: N-(diphenylphosphino)acetamide

: 835633-34-6
[Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2NC(O)Me)]

Guidance literature:: With KO-t-Bu; In tetrahydrofuran; byproducts: KCl, t-BuOH; (N2); std. Schlenk technique; mixt. of PPh2NHC(O)Me (1 equiv.), Pd complex (0.5 equiv.) and KO-t-Bu (1 equiv.) in THF was stirred overnight; solvent removed (vac.); extd. (CH2Cl2);
DOI:10.1021/om050156d

Reference yield: 88.0%

: tetrakis(acetonitrile)copper(I)tetrafluoroborate

: 835633-34-6
[Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2NC(O)Me)]

: 857686-05-6
[(Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2N(O)Me))2Cu]BF4

Guidance literature:: In tetrahydrofuran; byproducts: NCMe; (N2); std. Schlenk technique; Cu complex was added to soln. of Pd complex (2 equiv.) in THF; mixt. was stirred for 2 h; filtered; residue washed (THF); dried (vac.); elem. anal.;
DOI:10.1021/om050156d

Reference yield: 77.0%

: 14104-20-2
silver tetrafluoroborate

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 75-09-2
dichloromethane

: 835633-34-6
[Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2NC(O)Me)]

: [(Pd(dimethylbenzylamine(-1H))(κ2-P,O-PPh2N(O)Me))2Au]BF4*CH2Cl2

Guidance literature:: In tetrahydrofuran; dichloromethane; byproducts: SC4H8; (N2); std. Schlenk technique; solid AgBF4 was added to soln. of Au complex in CH2Cl2 at -60°C; filtered via cannula into soln. of Pd complex (2 equiv.) in THF at -60°C; mixt. was stirred for 3 h while warmed to room temp.; volatiles removed (vac.); residue washed (THF); dried (vac.); elem. anal.;
DOI:10.1021/om050156d