4-methoxyphenyltitanium triisopropoxide

Base Information

• Chemical Name: 4-methoxyphenyltitanium triisopropoxide
• CAS No.: 103594-89-4
• Molecular Formula: C₁₆H₂₈O₄Ti
• Molecular Weight: 332.276
• Mol file: 103594-89-4.mol

Synonyms:4-methoxyphenyltitanium triisopropoxide

Chemical Property of 4-methoxyphenyltitanium triisopropoxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-methoxyphenyltitanium triisopropoxide

There total 5 articles about 4-methoxyphenyltitanium triisopropoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

titanium(IV) isopropylate (546-68-9) + 4-methoxyphenylmagnesium chloride (699-19-4) → 4-methoxyphenyltitanium triisopropoxide (103594-89-4)

Guidance literature:

With titanium tetrachloride; In tetrahydrofuran; at -20 - 20 ℃; for 3.5h; Inert atmosphere;

DOI:10.1007/s00706-021-02796-6

Reference yield:

titanium(IV) isopropylate (546-68-9) + 1-bromo-4-methoxy-benzene (104-92-7) → 4-methoxyphenyltitanium triisopropoxide (103594-89-4)

Guidance literature:

1-bromo-4-methoxy-benzene; With magnesium; In tetrahydrofuran; for 3h; Inert atmosphere;

titanium(IV) isopropylate; With titanium tetrachloride; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c4ob00677a

Reference yield:

triisopropoxytitanium(IV) chloride (20717-86-6) + 1-bromo-4-methoxy-benzene (104-92-7) → 4-methoxyphenyltitanium triisopropoxide (103594-89-4)

Guidance literature:

1-bromo-4-methoxy-benzene; With n-butyllithium; In diethyl ether; hexane; at 0 - 20 ℃; for 0.166667h;

triisopropoxytitanium(IV) chloride; In diethyl ether; hexane; at 0 ℃; for 0.25h;

DOI:10.1002/chem.201701395

upstream raw materials:

titanium(IV) isopropylate

1-bromo-4-methoxy-benzene

triisopropoxytitanium(IV) chloride

para-iodoanisole

Downstream raw materials:

Estragole

BrTi(OiPr)3

4-methoxylphenylallene