(E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide

Base Information

Chemical Name:(E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide
CAS No.:1613246-83-5
Molecular Formula:C₂₂H₁₉N₃O₄S
Molecular Weight:421.477
Hs Code.:

Synonyms:(E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide

Suppliers and Price of (E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide

Chemical Property:

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Technology Process of (E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide

There total 5 articles about (E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 6655-77-2
3-nitrophenylsulfonohydrazide

: 62326-47-0
1,3-diphenyl-3-buten-1-one

: 1613246-83-5
(E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide

Guidance literature:: With ethanol; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol5013982

Reference yield:

: 3360-54-1
3-bromo-2-phenylprop-1-ene

: 1613246-83-5
(E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; water / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 3 h / 0 °C / Inert atmosphere

3: ethanol / 48 h / 20 °C / Inert atmosphere

With ethanol; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol5013982

Reference yield:

: 98-86-2
acetophenone

: 1613246-83-5
(E)-N'-(1,3-diphenylbut-3-en-1-ylidene)-3-nitrobenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium tert-butylate / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

2: N-Bromosuccinimide; toluene-4-sulfonic acid / 4 h / 100 °C / Inert atmosphere

3: tetrahydrofuran; water / Inert atmosphere

4: Dess-Martin periodane / dichloromethane / 3 h / 0 °C / Inert atmosphere

5: ethanol / 48 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; ethanol; potassium tert-butylate; Dess-Martin periodane; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol5013982