4-METHYL-6-PHENYLPYRIMIDIN-2-AMINE

Base Information

• Chemical Name: 4-METHYL-6-PHENYLPYRIMIDIN-2-AMINE
• CAS No.: 15755-15-4
• Molecular Formula: C11H11 N3
• Molecular Weight: 185.228
• Hs Code.: 2933599090
• Mol file: 15755-15-4.mol

Synonyms:Pyrimidine,2-amino-4-methyl-6-phenyl- (6CI,8CI); 2-Amino-4-methyl-6-phenylpyrimidine;4-Methyl-6-phenyl-2-pyrimidinamine

Chemical Property of 4-METHYL-6-PHENYLPYRIMIDIN-2-AMINE

Chemical Property:

• Vapor Pressure: 1.31E-06mmHg at 25°C
• Refractive Index: 1.619
• Boiling Point: 400ºC at 760 mmHg
• Flash Point: 224.5ºC
• PSA: 51.80000
• Density: 1.159g/cm3
• LogP: 2.61540

Purity/Quality:

99%, ^*data from raw suppliers

4-Methyl-6-phenylpyrimidin-2-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-METHYL-6-PHENYLPYRIMIDIN-2-AMINE

There total 17 articles about 4-METHYL-6-PHENYLPYRIMIDIN-2-AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

CYANAMID (420-04-2) + (2Z)-3-amino-1-phenylbut-2-en-1-one (23652-90-6) → 2-amino-6-methyl-4-phenylpyrimidine (15755-15-4)

Guidance literature:

In water; for 6h; Heating;

Reference yield: 90.0%

guanidine hydrochloride (50-01-1) + 1-phenylbutan-1,3-dione (93-91-4) → 2-amino-6-methyl-4-phenylpyrimidine (15755-15-4)

Guidance literature:

With potassium carbonate; for 0.0333333h; microwave irradiation;

DOI:10.1071/CH06388

Reference yield: 78.0%

guanidine nitrate (113-00-8) + 1-phenylbutan-1,3-dione (93-91-4) → 2-amino-6-methyl-4-phenylpyrimidine (15755-15-4)

Guidance literature:

In ethanol; at 78 ℃; for 8h;

DOI:10.1016/j.bmc.2007.02.044

upstream raw materials:

guanidine nitrate

1-phenylbutan-1,3-dione

diguanidine carbonate

CYANAMID

Downstream raw materials:

N-acetyl-sulfanilic acid-(4-methyl-6-phenyl-pyrimidin-2-ylamide)

2-amino-6-methyl-4-phenylpyrimidine 1-oxide

2-chloro-6-methyl-4-phenylpyrimidine 1-oxide

5-iodo-4-methyl-6-phenyl-2-pyrimidinamine

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