28-(Phenylsulfonyl)-1-(trimethylsilyl)-1,4,7,10,13,16,19,22,25,28-decaoxaoctacosane

Base Information

Chemical Name:28-(Phenylsulfonyl)-1-(trimethylsilyl)-1,4,7,10,13,16,19,22,25,28-decaoxaoctacosane
CAS No.:86217-84-7
Molecular Formula:C₂₇H₅₀O₁₂SSi
Molecular Weight:626.838
Hs Code.:

Synonyms:28-(Phenylsulfonyl)-1-(trimethylsilyl)-1,4,7,10,13,16,19,22,25,28-decaoxaoctacosane

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Chemical Property of 28-(Phenylsulfonyl)-1-(trimethylsilyl)-1,4,7,10,13,16,19,22,25,28-decaoxaoctacosane

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Technology Process of 28-(Phenylsulfonyl)-1-(trimethylsilyl)-1,4,7,10,13,16,19,22,25,28-decaoxaoctacosane

There total 3 articles about 28-(Phenylsulfonyl)-1-(trimethylsilyl)-1,4,7,10,13,16,19,22,25,28-decaoxaoctacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 75-77-4
chloro-trimethyl-silane

: Benzenesulfonic acid 2-[2-(2-{2-[2-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl ester

: 86217-84-7
28-(Phenylsulfonyl)-1-(trimethylsilyl)-1,4,7,10,13,16,19,22,25,28-decaoxaoctacosane

Guidance literature:: In dichloromethane; at 25 ℃; for 2h;
DOI:10.1021/jo00164a006

Reference yield:

: 3386-18-3
nonaethylene glycol

: 86217-84-7
28-(Phenylsulfonyl)-1-(trimethylsilyl)-1,4,7,10,13,16,19,22,25,28-decaoxaoctacosane

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / CH₂Cl₂; pyridine / 0 °C

2: 98 percent / CH₂Cl₂ / 2 h / 25 °C

In pyridine; dichloromethane;
DOI:10.1021/jo00164a006

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 86217-84-7
28-(Phenylsulfonyl)-1-(trimethylsilyl)-1,4,7,10,13,16,19,22,25,28-decaoxaoctacosane

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / CH₂Cl₂; pyridine / 0 °C

2: 98 percent / CH₂Cl₂ / 2 h / 25 °C

In pyridine; dichloromethane;
DOI:10.1021/jo00164a006