5-(4-methoxyphenyl)-5-(3-methylbut-2-enyl)-3-phenylmethyl-2,4-imidazolidinedione

Base Information

Chemical Name:5-(4-methoxyphenyl)-5-(3-methylbut-2-enyl)-3-phenylmethyl-2,4-imidazolidinedione
CAS No.:1443523-50-9
Molecular Formula:C₂₂H₂₄N₂O₃
Molecular Weight:364.444
Hs Code.:

Synonyms:5-(4-methoxyphenyl)-5-(3-methylbut-2-enyl)-3-phenylmethyl-2,4-imidazolidinedione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-methoxyphenyl)-5-(3-methylbut-2-enyl)-3-phenylmethyl-2,4-imidazolidinedione

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Technology Process of 5-(4-methoxyphenyl)-5-(3-methylbut-2-enyl)-3-phenylmethyl-2,4-imidazolidinedione

There total 3 articles about 5-(4-methoxyphenyl)-5-(3-methylbut-2-enyl)-3-phenylmethyl-2,4-imidazolidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1443523-44-1
3-benzyl-5-(4-methoxyphenyl)hydantoin

: 78-79-5,9003-31-0
isoprene

: 1443523-50-9
5-(4-methoxyphenyl)-5-(3-methylbut-2-enyl)-3-phenylmethyl-2,4-imidazolidinedione

Guidance literature:: With dodecacarbonyl-triangulo-triruthenium; bis(2-diphenylphosphinoethyl)phenylphosphine; In tetrahydrofuran; at 140 ℃; for 48h; Inert atmosphere; Sealed tube;
DOI:10.1039/c3cc43463j

Reference yield:

: 6617-78-3
5-(4-methoxyphenyl)imidazolidone-2,4-dione

: 1443523-50-9
5-(4-methoxyphenyl)-5-(3-methylbut-2-enyl)-3-phenylmethyl-2,4-imidazolidinedione

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0 °C

1.2: 18 h / 20 °C

2.1: dodecacarbonyl-triangulo-triruthenium; bis(2-diphenylphosphinoethyl)phenylphosphine / tetrahydrofuran / 48 h / 140 °C / Inert atmosphere; Sealed tube

With dodecacarbonyl-triangulo-triruthenium; potassium carbonate; bis(2-diphenylphosphinoethyl)phenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c3cc43463j

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1443523-50-9
5-(4-methoxyphenyl)-5-(3-methylbut-2-enyl)-3-phenylmethyl-2,4-imidazolidinedione

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol; water / 18 h / 60 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0 °C

2.2: 18 h / 20 °C

3.1: dodecacarbonyl-triangulo-triruthenium; bis(2-diphenylphosphinoethyl)phenylphosphine / tetrahydrofuran / 48 h / 140 °C / Inert atmosphere; Sealed tube

With dodecacarbonyl-triangulo-triruthenium; potassium carbonate; bis(2-diphenylphosphinoethyl)phenylphosphine; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc43463j