(5R,6S)-3-acetyl-5-(acetyloxy)methyl-2-methyl-1-phenyl-1,5,6,7-tetrahydropyrano[3,2-b]pyrrol-6-yl acetate

Base Information

Chemical Name:(5R,6S)-3-acetyl-5-(acetyloxy)methyl-2-methyl-1-phenyl-1,5,6,7-tetrahydropyrano[3,2-b]pyrrol-6-yl acetate
CAS No.:1020540-81-1
Molecular Formula:C₂₁H₂₃NO₆
Molecular Weight:385.417
Hs Code.:

Synonyms:(5R,6S)-3-acetyl-5-(acetyloxy)methyl-2-methyl-1-phenyl-1,5,6,7-tetrahydropyrano[3,2-b]pyrrol-6-yl acetate

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Chemical Property of (5R,6S)-3-acetyl-5-(acetyloxy)methyl-2-methyl-1-phenyl-1,5,6,7-tetrahydropyrano[3,2-b]pyrrol-6-yl acetate

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Technology Process of (5R,6S)-3-acetyl-5-(acetyloxy)methyl-2-methyl-1-phenyl-1,5,6,7-tetrahydropyrano[3,2-b]pyrrol-6-yl acetate

There total 4 articles about (5R,6S)-3-acetyl-5-(acetyloxy)methyl-2-methyl-1-phenyl-1,5,6,7-tetrahydropyrano[3,2-b]pyrrol-6-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: C₁₇H₁₉NO₄

: 108-24-7
acetic anhydride

: 1020540-81-1
(5R,6S)-3-acetyl-5-(acetyloxy)methyl-2-methyl-1-phenyl-1,5,6,7-tetrahydropyrano[3,2-b]pyrrol-6-yl acetate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 0.5h; Green chemistry;
DOI:10.1039/c4ra14379e

Reference yield: 93.0%

: 50-99-7
D-glucose

: 108-24-7
acetic anhydride

: 62-53-3
aniline

: 123-54-6,81235-32-7
acetylacetone

: 1020540-81-1
(5R,6S)-3-acetyl-5-(acetyloxy)methyl-2-methyl-1-phenyl-1,5,6,7-tetrahydropyrano[3,2-b]pyrrol-6-yl acetate

Guidance literature:: D-glucose; aniline; acetylacetone; With indium(III) chloride; In water; at 80 ℃; for 6h;

acetic anhydride; With dmap; In dichloromethane; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/jo702012w

Reference yield: 47.0%

: 108-24-7
acetic anhydride

: 62-53-3
aniline

: 123-54-6,81235-32-7
acetylacetone

: 57-50-1
Sucrose

: 1020540-81-1
(5R,6S)-3-acetyl-5-(acetyloxy)methyl-2-methyl-1-phenyl-1,5,6,7-tetrahydropyrano[3,2-b]pyrrol-6-yl acetate

Guidance literature:: aniline; acetylacetone; Sucrose; With indium(III) chloride; In water; at 80 ℃; for 7.5h;

acetic anhydride; With dmap; In dichloromethane; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/jo702012w